1-Hexanol, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[2-[[(1,1-dimethylethyl)dimethyl silyl]oxy]ethyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

Base Information

Chemical Name:1-Hexanol, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[2-[[(1,1-dimethylethyl)dimethyl silyl]oxy]ethyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-
CAS No.:837364-65-5
Molecular Formula:C27H53NO4Si2
Molecular Weight:511.893
Hs Code.:

1-Hexanol,
6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[2-[[(1,1-dimethylethyl)dimethyl
silyl]oxy]ethyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

Synonyms:

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Chemical Property of 1-Hexanol, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[2-[[(1,1-dimethylethyl)dimethyl silyl]oxy]ethyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Hexanol, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[2-[[(1,1-dimethylethyl)dimethyl silyl]oxy]ethyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

There total 2 articles about 1-Hexanol, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[2-[[(1,1-dimethylethyl)dimethyl silyl]oxy]ethyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87184-81-4
4-(tert-butyldimethylsilanyloxy)butanal

: 104-94-9
4-methoxy-aniline

: 6-(tert-butyldimethylsilyloxy)-2-[(2-tert-butyldimethylsilyloxy)ethyl]-3-(4-methoxyphenylamino)-hexan-1-ol

: 87184-99-4
4-tert-butyldimethylsilyloxybutan-1-ol

: 837364-65-5
(2S,3R)-6-(tert-butyldimethylsilyloxy)-2-[(2-tert-butyldimethylsilyloxy)ethyl]-3-(4-methoxyphenylamino)-hexan-1-ol

Guidance literature:: 4-(tert-butyldimethylsilanyloxy)butanal; 4-methoxy-aniline; With L-proline; In acetonitrile; at -40 - -30 ℃; for 26h;

With sodium tetrahydroborate; In diethyl ether; acetonitrile; at 0 ℃; for 0.25h;
DOI:10.1021/jo060130b

Reference yield:

: 6-(tert-butyl-dimethyl-silanyloxy)-2-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-3-(4-methoxy-phenylamino)-hexanal

: 6-(tert-butyl-dimethyl-silanyloxy)-2-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-3-(4-methoxy-phenylamino)-hexan-1-ol

: 837364-65-5
(2S,3R)-6-(tert-butyldimethylsilyloxy)-2-[(2-tert-butyldimethylsilyloxy)ethyl]-3-(4-methoxyphenylamino)-hexan-1-ol

: 6-(tert-butyl-dimethyl-silanyloxy)-2-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-3-(4-methoxy-phenylamino)-hexan-1-ol

Guidance literature:: With sodium tetrahydroborate; In acetonitrile; at -40 ℃; Further Variations:; Solvents; Temperatures; Product distribution;
DOI:10.1055/s-2004-835622