4,12-Dioxa-3,13-disilapentadecan-8-amine, 7-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-N-(4-methoxyphenyl)-2,2, 3,3,13,13,14,14-octamethyl-, (7S,8R)-

Base Information

Chemical Name:4,12-Dioxa-3,13-disilapentadecan-8-amine, 7-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-N-(4-methoxyphenyl)-2,2, 3,3,13,13,14,14-octamethyl-, (7S,8R)-
CAS No.:837364-67-7
Molecular Formula:C43H71NO4Si3
Molecular Weight:750.298
Hs Code.:

4,12-Dioxa-3,13-disilapentadecan-8-amine,
7-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-N-(4-methoxyphenyl)-2,2,
3,3,13,13,14,14-octamethyl-, (7S,8R)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,12-Dioxa-3,13-disilapentadecan-8-amine, 7-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-N-(4-methoxyphenyl)-2,2, 3,3,13,13,14,14-octamethyl-, (7S,8R)-

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Technology Process of 4,12-Dioxa-3,13-disilapentadecan-8-amine, 7-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-N-(4-methoxyphenyl)-2,2, 3,3,13,13,14,14-octamethyl-, (7S,8R)-

There total 1 articles about 4,12-Dioxa-3,13-disilapentadecan-8-amine, 7-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-N-(4-methoxyphenyl)-2,2, 3,3,13,13,14,14-octamethyl-, (7S,8R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 837364-65-5
(2S,3R)-6-(tert-butyldimethylsilyloxy)-2-[(2-tert-butyldimethylsilyloxy)ethyl]-3-(4-methoxyphenylamino)-hexan-1-ol

: 837364-67-7
[4-(tert-butyl-dimethyl-silanyloxy)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(tert-butyl-diphenyl-silanyloxymethyl)-butyl]-(4-methoxy-phenyl)-amine

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1055/s-2004-835622

Reference yield: 91.0%

: 837364-67-7
[4-(tert-butyl-dimethyl-silanyloxy)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(tert-butyl-diphenyl-silanyloxymethyl)-butyl]-(4-methoxy-phenyl)-amine

: 837364-68-8
(3S,4R)-3-(tert-butyldiphenylsilyloxy)methyl-4-(4-methoxyphenylamino)-heptane-1,7-diol

Guidance literature:: With toluene-4-sulfonic acid; In methanol;
DOI:10.1055/s-2004-835622

Reference yield:

: 837364-67-7
[4-(tert-butyl-dimethyl-silanyloxy)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(tert-butyl-diphenyl-silanyloxymethyl)-butyl]-(4-methoxy-phenyl)-amine

: (2R,3S)-3-(tert-butyldiphenylsilyloxymethyl)-1-(4-methoxyphenyl)-2-(3-hydroxypropyl)-pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1.33 g / p-toluenesulfonic acid / methanol / 20 °C

2.1: C₁,1'-carbonyldiimidazole / acetonitrile / 2 h / Heating

2.2: 69 percent / aq. NaOH / tetrahydrofuran / 2 h / 20 °C

With toluene-4-sulfonic acid; 1,1'-carbonyldiimidazole; In methanol; acetonitrile;
DOI:10.1021/jo060130b