1-Heptanol, 7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[3-[[(1,1-dimethylethyl)dimethyl silyl]oxy]propyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

Base Information

Chemical Name:1-Heptanol, 7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[3-[[(1,1-dimethylethyl)dimethyl silyl]oxy]propyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-
CAS No.:837364-75-7
Molecular Formula:C₂₉H₅₇NO₄Si₂
Molecular Weight:539.947
Hs Code.:

1-Heptanol,
7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[3-[[(1,1-dimethylethyl)dimethyl
silyl]oxy]propyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

Synonyms:

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Chemical Property of 1-Heptanol, 7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[3-[[(1,1-dimethylethyl)dimethyl silyl]oxy]propyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

Chemical Property:

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Technology Process of 1-Heptanol, 7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[3-[[(1,1-dimethylethyl)dimethyl silyl]oxy]propyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)-

There total 1 articles about 1-Heptanol, 7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-[3-[[(1,1-dimethylethyl)dimethyl silyl]oxy]propyl]-3-[(4-methoxyphenyl)amino]-, (2S,3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87184-80-3
5-tert-butyldimethylsilyloxypentanal

: 104-94-9
4-methoxy-aniline

: 6-(tert-butyldimethylsilyloxy)-2-[(3-tert-butyldimethylsilyloxy)propyl]-3-(4-methoxyphenylamino)-heptan-ol

: 837364-75-7
(2S,3R)-6-(tert-butyldimethylsilyloxy)-2-[(3-tert-butyldimethylsilyloxy)propyl]-3-(4-methoxyphenylamino)-heptan-ol

Guidance literature:: 5-tert-butyldimethylsilyloxypentanal; 4-methoxy-aniline; With L-proline; In acetonitrile; at -40 - -30 ℃; for 26h;

With sodium tetrahydroborate; In diethyl ether; acetonitrile; at 0 ℃; for 0.25h;
DOI:10.1021/jo060130b

Reference yield:

: 837364-75-7
(2S,3R)-6-(tert-butyldimethylsilyloxy)-2-[(3-tert-butyldimethylsilyloxy)propyl]-3-(4-methoxyphenylamino)-heptan-ol

: (2R,3R)-2-(4-(tert-butyldimethylsilyloxy)butyl)-3-(3-(tert-butyldimethylsilyloxy)propyl)-1-(4-methoxyphenyl)azetidine

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 12 h / Heating

2: 2 h / 150 °C / 0.08 Torr

In acetonitrile;
DOI:10.1021/jo060130b