7,7-Dichloro-2-oxabicyclo[4.1.0]heptane

Base Information

Chemical Name:7,7-Dichloro-2-oxabicyclo[4.1.0]heptane
CAS No.:7556-13-0
Molecular Formula:C6H8Cl2O
Molecular Weight:167.0331
Hs Code.:
NSC Number:130991
DSSTox Substance ID:DTXSID40299471,DTXSID00872062
Nikkaji Number:J81.418K
Mol file:7556-13-0.mol

Synonyms:7,7-dichloro-2-oxabicyclo[4.1.0]heptane;7556-13-0;7,7-dichloro-5-oxabicyclo[4.1.0]heptane;NSC130991;7,7-dichloro-2-oxa-bicyclo[4.1.0]heptane;CERAPP_64358;SCHEMBL11774560;DTXSID00872062;DTXSID40299471;NSC-130991;7,7-dichloro-2-oxabicyclo[4,1,0]heptane;FT-0655196;2-Oxabicyclo[4.1.0]heptane, 7,7-dichloro-;A19140

Suppliers and Price of 7,7-Dichloro-2-oxabicyclo[4.1.0]heptane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
7,7-DICHLORO-2-OXABICYCLO[4.1.0]HEPTANE 95.00%
10G
$ 1334.03

American Custom Chemicals Corporation
7,7-DICHLORO-2-OXABICYCLO[4.1.0]HEPTANE 95.00%
5G
$ 909.56

Total 8 raw suppliers

Chemical Property of 7,7-Dichloro-2-oxabicyclo[4.1.0]heptane

Chemical Property:

Vapor Pressure:0.0724mmHg at 25°C
Boiling Point:236.5°Cat760mmHg
Flash Point:144.9°C
PSA：9.23000
Density:1.37g/cm³
LogP:1.96910
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:165.9952203
Heavy Atom Count:9
Complexity:135

Purity/Quality:

97% ^*data from raw suppliers

7,7-DICHLORO-2-OXABICYCLO[4.1.0]HEPTANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2C(C2(Cl)Cl)OC1

Technology Process of 7,7-Dichloro-2-oxabicyclo[4.1.0]heptane

There total 3 articles about 7,7-Dichloro-2-oxabicyclo[4.1.0]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 56-23-5
tetrachloromethane

: 7556-13-0
7,7-dichloro-2-oxa-bicyclo[4.1.0]heptane

Guidance literature:: With magnesium; In tetrahydrofuran; diethyl ether; at 20 ℃; ultrasonic irradiation;
DOI:10.3390/80800608

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 67-66-3,8013-54-5
chloroform

: 7556-13-0
7,7-dichloro-2-oxa-bicyclo[4.1.0]heptane

Guidance literature:: With sodium hydroxide; α,α'-bis(triethyl ammonium methylene chloride) β-phenyl ethene; Yield given. Multistep reaction; 1.) 45 deg C, 10 min, 2.) 24 min;
DOI:10.1080/00397919508011456

Reference yield:

: 7556-13-0
7,7-dichloro-2-oxa-bicyclo[4.1.0]heptane

Guidance literature:: 1 Mol wssfr.Dihydropyran/Pentan <0-5grad>, 1.1 Mol Trichloressigsaeureethylester, NaOCH3 (1.15 Mol) ;
DOI:10.1021/ja01500a064