3-benzo[1,3]dioxol-4-ylpropanoic acid

Base Information

Chemical Name:3-benzo[1,3]dioxol-4-ylpropanoic acid
CAS No.:20974-68-9
Molecular Formula:C10H10 O4
Molecular Weight:194.18
Hs Code.:2932999099
Mol file:20974-68-9.mol

Synonyms:Hydrocinnamicacid, 2,3-(methylenedioxy)- (8CI); NSC 28957

Suppliers and Price of 3-benzo[1,3]dioxol-4-ylpropanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-(2H-1,3-benzodioxol-4-yl)propanoicAcid
10mg
$ 45.00

AK Scientific
3-(1,3-Benzodioxol-4-yl)propanoicacid
5g
$ 2332.00

AK Scientific
3-(1,3-Benzodioxol-4-yl)propanoicacid
100mg
$ 328.00

Total 4 raw suppliers

Chemical Property of 3-benzo[1,3]dioxol-4-ylpropanoic acid

Chemical Property:

Vapor Pressure:1.27E-05mmHg at 25°C
Melting Point:80-82 °C
Boiling Point:354°Cat760mmHg
PKA:4.56±0.10(Predicted)
Flash Point:144.1°C
PSA：55.76000
Density:1.343g/cm³
LogP:1.43250

Purity/Quality:

99% ^*data from raw suppliers

3-(2H-1,3-benzodioxol-4-yl)propanoicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-benzo[1,3]dioxol-4-ylpropanoic acid

There total 4 articles about 3-benzo[1,3]dioxol-4-ylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 287118-44-9
3-(2,3-methylenedioxyphenyl)acrylic acid

: 20974-68-9
3-<2,3-(methylenedioxy)phenyl>propanoic acid

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 20h; Sealed tube;
DOI:10.1021/acs.orglett.1c02767

Reference yield: 90.0%

: 38489-70-2
2,3-(methylenedioxy)cinnamic acid

: 20974-68-9
3-<2,3-(methylenedioxy)phenyl>propanoic acid

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; water; at 20 ℃; for 3h; under 3102.97 Torr;

Reference yield:

: 7797-83-3
2H-benzo[d]1,3-dioxolane-4-carbaldehyde

: 20974-68-9
3-<2,3-(methylenedioxy)phenyl>propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 0.5 h / 80 - 85 °C

1.2: 3 h / Heating

2.1: H₂ / Pd-C / ethanol / 5 h / 3102.89 Torr

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; 1.1: Condensation / 1.2: Decarboxylation / 2.1: Hydrogenation;
DOI:10.1016/S0968-0896(00)00048-1