Ethanone, 1-phenyl-, O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)prop yl]oxime, (1E)-

Base Information

Chemical Name:Ethanone, 1-phenyl-, O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)prop yl]oxime, (1E)-
CAS No.:847435-66-9
Molecular Formula:C22H29N5O
Molecular Weight:379.505
Hs Code.:

Synonyms:

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Chemical Property of Ethanone, 1-phenyl-, O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)prop yl]oxime, (1E)-

Chemical Property:

Purity/Quality:

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Technology Process of Ethanone, 1-phenyl-, O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)prop yl]oxime, (1E)-

There total 7 articles about Ethanone, 1-phenyl-, O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)prop yl]oxime, (1E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 847436-27-5
1-[3-(aminooxy)propyl]-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-4-amine

: 98-86-2
acetophenone

: (1Z)-1-phenylethanone O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)propyl]oxime

: 847435-66-9
(1E)-1-phenylethanone O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)propyl]oxime

Guidance literature:: With pyridine hydrochloride; In methanol; at 20 - 50 ℃; Heating / reflux;

Reference yield:

: 437384-55-9
2,4-Dichloro-5,6-Dimethyl-3-nitro-pyridine

: (1Z)-1-phenylethanone O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)propyl]oxime

: 847435-66-9
(1E)-1-phenylethanone O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)propyl]oxime

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / N,N-dimethyl-formamide / 16 h / 20 °C

2.1: sodium azide; cerium(III) chloride / water; acetonitrile / 16 h / Heating / reflux

3.1: hydrogen / palladium 10% on activated carbon / acetonitrile / 16 h / 2585.81 Torr

4.1: pyridine hydrochloride / toluene / 16 h / Heating / reflux

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / N,N-dimethyl-formamide / 4 h / 20 °C

6.1: triphenylphosphine / 1,2-dichloro-benzene / 120 h / 20 - 125 °C

6.2: 5 h / 50 °C

7.1: pyridine hydrochloride / methanol / 20 - 50 °C / Heating / reflux

With sodium azide; cerium(III) chloride; di-isopropyl azodicarboxylate; hydrogen; pyridine hydrochloride; triethylamine; triphenylphosphine; palladium 10% on activated carbon; In methanol; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene; acetonitrile;

Reference yield:

: 634927-05-2
3-[(2-chloro-5,6-dimethyl-3-nitropyridin-4-yl)amino]propan-1-ol

: (1Z)-1-phenylethanone O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)propyl]oxime

: 847435-66-9
(1E)-1-phenylethanone O-[3-(4-amino-6,7-dimethyl-2-propyl-1H-imidazo[4,5-c]pyridin-1-yl)propyl]oxime

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide; cerium(III) chloride / water; acetonitrile / 16 h / Heating / reflux

2.1: hydrogen / palladium 10% on activated carbon / acetonitrile / 16 h / 2585.81 Torr

3.1: pyridine hydrochloride / toluene / 16 h / Heating / reflux

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / N,N-dimethyl-formamide / 4 h / 20 °C

5.1: triphenylphosphine / 1,2-dichloro-benzene / 120 h / 20 - 125 °C

5.2: 5 h / 50 °C

6.1: pyridine hydrochloride / methanol / 20 - 50 °C / Heating / reflux

With sodium azide; cerium(III) chloride; di-isopropyl azodicarboxylate; hydrogen; pyridine hydrochloride; triphenylphosphine; palladium 10% on activated carbon; In methanol; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene; acetonitrile;