2-(2-(2-Methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione

Base Information

Chemical Name:2-(2-(2-Methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione
CAS No.:84764-41-0
Molecular Formula:C₁₄H₁₅NO₄
Molecular Weight:261.277
Hs Code.:
DSSTox Substance ID:DTXSID30516725
Wikidata:Q82378272

Synonyms:84764-41-0;2-(2-(2-Methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione;2-[2-(2-Methyl-1,3-dioxolan-2-yl)ethyl]isoindoline-1,3-dione;2-[2-(2-METHYL-1,3-DIOXOLAN-2-YL)ETHYL]ISOINDOLE-1,3-DIONE;MFCD09923388;2-[2-(2-methyl-1,3-dioxolan-2-yl)ethyl]-2,3-dihydro-1H-isoindole-1,3-dione;SCHEMBL14821604;DTXSID30516725;2-[2-(2-Methyl-1,3-dioxolan-2-yl)ethyl]-1H-isoindole-1,3(2H)-dione;AKOS027255648;AS-70966;SY026749;CS-0153761;W10741;A914961

Suppliers and Price of 2-(2-(2-Methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2-(2-(2-Methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:261.10010796
Heavy Atom Count:19
Complexity:365

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(OCCO1)CCN2C(=O)C3=CC=CC=C3C2=O

Technology Process of 2-(2-(2-Methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione

There total 4 articles about 2-(2-(2-Methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3783-77-5
N-(3-oxobutyl)phthalimide

: 107-21-1
ethylene glycol

: 84764-41-0
2-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 3h; Inert atmosphere; Reflux; Dean-Stark;
DOI:10.1002/chem.202004455

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 84764-41-0
2-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: triton B / ethyl acetate / Heating

2: PTSA / toluene / Heating

With N-benzyl-trimethylammonium hydroxide; toluene-4-sulfonic acid; In ethyl acetate; toluene;

Reference yield:

: 1074-82-4
potassium phtalimide

: 84764-41-0
2-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / dimethylformamide / 32 h / Heating

2: 72 percent / toluene-p-sulphonic acid (PTSA) / benzene / 48 h / Heating

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; benzene;