methyl-2,4-diamino-2,4-dideoxy-6-O-(2,6-diamino-2,6-dideoxy-alpha-D-glucopyranosyl)-beta-D-glucopyranoside

Base Information

Chemical Name:methyl-2,4-diamino-2,4-dideoxy-6-O-(2,6-diamino-2,6-dideoxy-alpha-D-glucopyranosyl)-beta-D-glucopyranoside
CAS No.:86327-82-4
Molecular Formula:C₁₃H₂₈N₄O₇
Molecular Weight:352.388
Hs Code.:

Synonyms:methyl-2,4-diamino-2,4-dideoxy-6-O-(2,6-diamino-2,6-dideoxy-alpha-D-glucopyranosyl)-beta-D-glucopyranoside

Suppliers and Price of methyl-2,4-diamino-2,4-dideoxy-6-O-(2,6-diamino-2,6-dideoxy-alpha-D-glucopyranosyl)-beta-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl-2,4-diamino-2,4-dideoxy-6-O-(2,6-diamino-2,6-dideoxy-alpha-D-glucopyranosyl)-beta-D-glucopyranoside

Chemical Property:

PSA：201.69000
LogP:-2.07630

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl-2,4-diamino-2,4-dideoxy-6-O-(2,6-diamino-2,6-dideoxy-alpha-D-glucopyranosyl)-beta-D-glucopyranoside

There total 7 articles about methyl-2,4-diamino-2,4-dideoxy-6-O-(2,6-diamino-2,6-dideoxy-alpha-D-glucopyranosyl)-beta-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 86319-54-2
Methyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-6-O-(2,6-diazido-3,4-di-O-benzyl-2,6-desoxy-α-D-glucopyranosyl)-β-D-glucopyranosid

: 86327-82-4
Methyl-2,4-diamino-2,4-didesoxy-6-O-(2,6-diamino-2,6-didesoxy-α-D-glucopyranosyl)-β-D-glucopyranosid

Guidance literature:: With tetrahydrofuran; ammonia; sodium; Heating;
DOI:10.1016/S0008-6215(00)90950-9

Reference yield:

: 61135-12-4
6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

: 86327-82-4
Methyl-2,4-diamino-2,4-didesoxy-6-O-(2,6-diamino-2,6-didesoxy-α-D-glucopyranosyl)-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / molecular sieve, silver carbonate / CH₂Cl₂ / 0.08 h

2: 97 percent / sodium methoxide / methanol / 0.5 h / Heating

3: 1.) mercury (II) bromide, molecular sieve / 1.) CH₂Cl₂, 1 h, r.t.; 2.) CH₂Cl₂, -40 deg C, 6.5 h

4: 99 percent / sodium methanolate / methanol / 0.5 h / Heating

5: 501 mg / pyridine / 6 h / 0 °C

6: sodium azide / dimethylformamide / 1 h / 90 °C

7: 24 percent / liq. ammonia, sodium, oxolane / Heating

With tetrahydrofuran; sodium azide; molecular sieve; ammonia; sodium methylate; sodium; silver carbonate; mercury dibromide; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90950-9

Reference yield:

: 86319-52-0
Methyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

: 86327-82-4
Methyl-2,4-diamino-2,4-didesoxy-6-O-(2,6-diamino-2,6-didesoxy-α-D-glucopyranosyl)-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) mercury (II) bromide, molecular sieve / 1.) CH₂Cl₂, 1 h, r.t.; 2.) CH₂Cl₂, -40 deg C, 6.5 h

2: 99 percent / sodium methanolate / methanol / 0.5 h / Heating

3: 501 mg / pyridine / 6 h / 0 °C

4: sodium azide / dimethylformamide / 1 h / 90 °C

5: 24 percent / liq. ammonia, sodium, oxolane / Heating

With tetrahydrofuran; sodium azide; molecular sieve; ammonia; sodium methylate; sodium; mercury dibromide; In pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90950-9