6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

Base Information

Chemical Name:6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid
CAS No.:61135-12-4
Molecular Formula:C₁₅H₁₇BrN₆O₄
Molecular Weight:425.242
Hs Code.:

Synonyms:6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

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Chemical Property of 6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

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Technology Process of 6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

There total 1 articles about 6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61135-12-4
6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

Guidance literature:: Diacetat 3, HBr;
DOI:10.1016/S0008-6215(00)83775-1

Reference yield: 81.0%

: 67-56-1
methanol

: 61135-12-4
6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

: 86319-51-9
Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Guidance literature:: With molecular sieve; silver carbonate; In dichloromethane; for 0.0833333h;
DOI:10.1016/S0008-6215(00)90950-9

Reference yield:

: 61135-12-4
6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

: 86319-53-1
Methyl-6-O-(6-O-Acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / molecular sieve, silver carbonate / CH₂Cl₂ / 0.08 h

2: 97 percent / sodium methoxide / methanol / 0.5 h / Heating

3: 1.) mercury (II) bromide, molecular sieve / 1.) CH₂Cl₂, 1 h, r.t.; 2.) CH₂Cl₂, -40 deg C, 6.5 h

With molecular sieve; sodium methylate; silver carbonate; mercury dibromide; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)90950-9