Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Base Information

Chemical Name:Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid
CAS No.:86319-51-9
Molecular Formula:C₁₆H₂₀N₆O₅
Molecular Weight:376.372
Hs Code.:

Synonyms:Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

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Technology Process of Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

There total 1 articles about Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67-56-1
methanol

: 61135-12-4
6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

: 86319-51-9
Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Guidance literature:: With molecular sieve; silver carbonate; In dichloromethane; for 0.0833333h;
DOI:10.1016/S0008-6215(00)90950-9

Reference yield: 97.0%

: 86319-51-9
Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

: 86319-52-0
Methyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Guidance literature:: With sodium methylate; In methanol; for 0.5h; Heating;
DOI:10.1016/S0008-6215(00)90950-9

Reference yield:

: 86319-51-9
Methyl 6-O-acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

: 86319-54-2
Methyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-6-O-(2,6-diazido-3,4-di-O-benzyl-2,6-desoxy-α-D-glucopyranosyl)-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / sodium methoxide / methanol / 0.5 h / Heating

2: 1.) mercury (II) bromide, molecular sieve / 1.) CH₂Cl₂, 1 h, r.t.; 2.) CH₂Cl₂, -40 deg C, 6.5 h

3: 99 percent / sodium methanolate / methanol / 0.5 h / Heating

4: 501 mg / pyridine / 6 h / 0 °C

5: sodium azide / dimethylformamide / 1 h / 90 °C

With sodium azide; molecular sieve; sodium methylate; mercury dibromide; In pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90950-9