Technology Process of Ethanol, 2-[(3-fluorophenyl)methoxy]-
There total 5 articles about Ethanol, 2-[(3-fluorophenyl)methoxy]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-((allyloxy)methyl)-3-fluorobenzene;
With
ruthenium trichloride; sodium periodate; N-benzyl-N,N,N-triethylammonium chloride;
In
ethyl acetate;
With
lithium borohydride; chloro-trimethyl-silane;
In
tetrahydrofuran;
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran;
at 60 ℃;
for 120h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere
1.2: 4 h / 0 °C / Inert atmosphere
2.1: ruthenium trichloride; N-benzyl-N,N,N-triethylammonium chloride; sodium periodate / water; ethyl acetate / 2 h / 20 °C / Inert atmosphere
3.1: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran / Inert atmosphere
With
ruthenium trichloride; sodium periodate; lithium borohydride; chloro-trimethyl-silane; N-benzyl-N,N,N-triethylammonium chloride; sodium hydride;
In
tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ml400381s