1-Methoxy-4-[(Z)-(4-methylphenyl)-NNO-azoxy]benzene

Base Information

Chemical Name:1-Methoxy-4-[(Z)-(4-methylphenyl)-NNO-azoxy]benzene
CAS No.:85314-04-1
Molecular Formula:C14H14N2O2
Molecular Weight:242.277
Hs Code.:
DSSTox Substance ID:DTXSID70516683

Synonyms:85314-04-1;1-Methoxy-4-[(Z)-(4-methylphenyl)-NNO-azoxy]benzene;DTXSID70516683

Suppliers and Price of 1-Methoxy-4-[(Z)-(4-methylphenyl)-NNO-azoxy]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methoxy-4-[(Z)-(4-methylphenyl)-NNO-azoxy]benzene

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:242.105527694
Heavy Atom Count:18
Complexity:278

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=[N+](C2=CC=C(C=C2)OC)[O-]

Technology Process of 1-Methoxy-4-[(Z)-(4-methylphenyl)-NNO-azoxy]benzene

There total 6 articles about 1-Methoxy-4-[(Z)-(4-methylphenyl)-NNO-azoxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.7%

: 99-99-0
1-methyl-4-nitrobenzene

: 21650-57-7
(E)-1-(4-methoxyphenyl)-2-(4-methylphenyl)diazene

: 85314-04-1
N-(4-Methoxy-phenyl)-N'-p-tolyl-diazene N'-oxide

: 501-60-0
(E)-4,4'-dimethylazobenzene

: 501-58-6,21650-55-5,82570-64-7
(E)-1,2-bis(4-methoxyphenyl)diazene

Guidance literature:: In tetrahydrofuran; at 55 ℃; for 3h;
DOI:10.1246/bcsj.62.915

Reference yield:

: 29418-44-8
1-(4-methoxyphenyl)-2-p-tolyldiazene

: 85314-04-1
4-methoxy-ONN-4'-methylazoxybenzene

: 85314-03-0
4-methoxy-NNO-4'-methylazoxybenzene

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 65 ℃; Yield given. Yields of byproduct given;
DOI:10.1246/bcsj.60.3814

Reference yield:

: 623-11-0
1-methyl-4-nitrosobenzene

: 85314-04-1
4-methoxy-ONN-4'-methylazoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 86.5 percent / acetic acid; ethanol / 0.5 h / 50 °C

2: 1.) 30percent H₂O₂; 2.) CrO₃ / 1.) acetic acid, 65 deg C; 2.) ethanol, 30-40 deg C, 30 min and 55-60 deg C, 3 h

With chromium(VI) oxide; dihydrogen peroxide; In ethanol; acetic acid;
DOI:10.1246/bcsj.60.3814