5-METHOXY-2-NITROPHENYLBORONIC ACID

Base Information

Chemical Name:5-METHOXY-2-NITROPHENYLBORONIC ACID
CAS No.:860033-98-3
Molecular Formula:C₇H₈BNO₅
Molecular Weight:196.955
Hs Code.:

Synonyms:

Suppliers and Price of 5-METHOXY-2-NITROPHENYLBORONIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
5-Methoxy-2-nitrophenylboronic acid 95%
10g
$ 3664.00

Matrix Scientific
5-Methoxy-2-nitrophenylboronic acid 95%
5g
$ 2590.00

Total 2 raw suppliers

Chemical Property of 5-METHOXY-2-NITROPHENYLBORONIC ACID

Chemical Property:

PSA：95.51000
LogP:-0.19360

Purity/Quality:

95%-98% ^*data from raw suppliers

5-Methoxy-2-nitrophenylboronic acid 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-METHOXY-2-NITROPHENYLBORONIC ACID

There total 4 articles about 5-METHOXY-2-NITROPHENYLBORONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 121-43-7,63156-11-6
Trimethyl borate

: 214279-40-0
3-iodo-4-nitroanisol

: 860033-98-3
(5-methoxy-2-nitrophenyl)boronic acid

Guidance literature:: 3-iodo-4-nitroanisol; With phenylmagnesium chloride; In tetrahydrofuran; at -78 ℃; for 0.5h;

Trimethyl borate; In tetrahydrofuran; at -78 ℃; for 0.5h;

hydrogenchloride; In tetrahydrofuran; water; at -20 ℃;
DOI:10.1002/ejoc.201900745

Reference yield: 79.0%

: 214279-40-0
3-iodo-4-nitroanisol

: 860033-98-3
(5-methoxy-2-nitrophenyl)boronic acid

Guidance literature:: 3-iodo-4-nitroanisol; With phenylmagnesium chloride; In tetrahydrofuran; at -60 ℃; for 0.0833333h;

With Trimethyl borate; In tetrahydrofuran; at -60 ℃; for 0.5h;

With hydrogenchloride; In tetrahydrofuran; at -20 ℃;
DOI:10.1016/j.tetlet.2005.04.129