Cyclohexanecarboxylic acid, 2-oxo-1-(phenylmethyl)-, 2-propenyl ester

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 2-oxo-1-(phenylmethyl)-, 2-propenyl ester
CAS No.:866105-65-9
Molecular Formula:C17H20O3
Molecular Weight:272.344
Hs Code.:

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Chemical Property of Cyclohexanecarboxylic acid, 2-oxo-1-(phenylmethyl)-, 2-propenyl ester

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Technology Process of Cyclohexanecarboxylic acid, 2-oxo-1-(phenylmethyl)-, 2-propenyl ester

There total 2 articles about Cyclohexanecarboxylic acid, 2-oxo-1-(phenylmethyl)-, 2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 91906-66-0
pimelic acid diallyl ester

: 100-39-0
benzyl bromide

: 866105-65-9
allyl 1-benzyl-2-oxocyclohexane-1-carboxylate

Guidance literature:: pimelic acid diallyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 40 ℃; for 18h;

benzyl bromide; In tetrahydrofuran; mineral oil; at 40 ℃; for 3h;
DOI:10.1002/anie.201606792

Reference yield: 70.0%

: 91906-66-0
pimelic acid diallyl ester

: 100-39-0
benzyl bromide

: 107-18-6
allyl alcohol

: 866105-65-9
allyl 1-benzyl-2-oxocyclohexane-1-carboxylate

Guidance literature:: allyl alcohol; With sodium hydride; In toluene; Inert atmosphere;

pimelic acid diallyl ester; In toluene; at 95 ℃; for 1h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 50 ℃; for 2.5h;
DOI:10.1002/chem.201003383

Reference yield: 99.0%

: 866105-65-9
allyl 1-benzyl-2-oxocyclohexane-1-carboxylate

: (S)-2-allyl-2-benzylcyclohexan-1-one

Guidance literature:: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; In tetrahydrofuran; at 25 ℃; for 0.5h; Product distribution / selectivity;