Benzoic acid, 2-(bromomethyl)-6-methoxy-, ethyl ester

Base Information

Chemical Name:Benzoic acid, 2-(bromomethyl)-6-methoxy-, ethyl ester
CAS No.:86823-81-6
Molecular Formula:C11H13BrO3
Molecular Weight:273.126
Hs Code.:

Synonyms:ethyl 3-O-methyl-6-bromomethylsalicylate;ethyl 2-(bromomethyl)-6-methoxybenzoate;2-bromomethyl-6-methoxy-benzoic acid ethyl ester;ethyl 2-bromomethyl-6-methoxybenzoate;2-Brommethyl-6-methoxybenzoesaeureethylester;2-(bromomethyl)-6-methoxybenzoic acid ethyl ester;

Suppliers and Price of Benzoic acid, 2-(bromomethyl)-6-methoxy-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Alichem
Ethyl2-bromomethyl-6-methoxybenzoate
1g
$ 1564.50

Alichem
Ethyl2-bromomethyl-6-methoxybenzoate
250mg
$ 470.40

Total 0 raw suppliers

Chemical Property of Benzoic acid, 2-(bromomethyl)-6-methoxy-, ethyl ester

Chemical Property:

PSA：35.53000
LogP:2.76680

Purity/Quality:: Ethyl2-bromomethyl-6-methoxybenzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzoic acid, 2-(bromomethyl)-6-methoxy-, ethyl ester

There total 3 articles about Benzoic acid, 2-(bromomethyl)-6-methoxy-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 6520-83-8
ethyl 2-methoxy-6-methylbenzoate

: 86823-81-6
6-bromomethyl-2-methoxy-benzoic acid ethyl ester

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 77 ℃; for 3h;
DOI:10.1021/ja0509984

Reference yield:

: 6555-40-4
ethyl 2-hydroxy-6-methylbenzoate

: 86823-81-6
6-bromomethyl-2-methoxy-benzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / potassium carbonate / acetone / 25 h / Heating

2: 93 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 8 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; potassium carbonate; In tetrachloromethane; acetone;
DOI:10.1016/S0040-4020(01)82406-6