(Pentafluorophenyl)(triethylgermyl)methanone

Base Information

Chemical Name:(Pentafluorophenyl)(triethylgermyl)methanone
CAS No.:86962-02-9
Molecular Formula:C₁₃H₁₅F₅GeO
Molecular Weight:354.844
Hs Code.:
DSSTox Substance ID:DTXSID60515428
Wikidata:Q82376300

Synonyms:(Pentafluorophenyl)(triethylgermyl)methanone;86962-02-9;DTXSID60515428

Suppliers and Price of (Pentafluorophenyl)(triethylgermyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Pentafluorophenyl)(triethylgermyl)methanone

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:356.0254837
Heavy Atom Count:20
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Ge](CC)(CC)C(=O)C1=C(C(=C(C(=C1F)F)F)F)F

Technology Process of (Pentafluorophenyl)(triethylgermyl)methanone

There total 2 articles about (Pentafluorophenyl)(triethylgermyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 6727-87-3
triethylgermyllithium

: 889-98-5
N,N-diethyl-2,3,4,5,6-pentafluorobenzamide

: 86962-02-9
(C₂H₅)3GeCOC₆F₅

: 86962-01-8
N,N-diethyl-2,4-bis(triethylgermyl)-3,5,6-trifluorobenzamide

Guidance literature:: With water; ammonium chloride; In hexane; in sealed evacuated ampule; soln. of Et3GeLi added to soln. of amide at-40°C; stirred at the same temp. for 3 h; hydrolyzed with satd. NH4Cl soln.; dried; isolated by fractionation of the dried org. part ; GLC; mass-spectrometry; elem. anal.;

Reference yield: 54.0%

: 6727-87-3
triethylgermyllithium

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: 86962-02-9
(C₂H₅)3GeCOC₆F₅

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; in sealed evacuated ampule; mixt. of Et3GeLi and CuI (equimol. amt.) inTHF stirred at -30°C for 30 min; pentafluorobenzoyl chloride added; stirred for 1 h while being gradually brought to room temp.; hexane added; ppt. filtered off; product isolated by fractionation of the yellow soln.; GLC; mass-spectrometry; NMR; elem. anal.;