6-Hydroxyhexyl acrylate

Base Information

• Chemical Name: 6-Hydroxyhexyl acrylate
• CAS No.: 10095-14-4
• Molecular Formula: C9H16O3
• Molecular Weight: 172.224
• Hs Code.: 2916129000
• European Community (EC) Number: 233-227-0
• DSSTox Substance ID: DTXSID20143589
• Nikkaji Number: J25.102J
• Wikidata: Q83007537
• Mol file: 10095-14-4.mol

Synonyms:6-Hydroxyhexyl acrylate;6-hydroxyhexyl prop-2-enoate;10095-14-4;EINECS 233-227-0;acrylic acid 6-hydroxyhexyl ester;HOHA;2-Propenoic acid, 6-hydroxyhexyl ester;1,6-hexanediol acrylate;6-hydroxyhexylprop-2-enoate;SCHEMBL57984;DTXSID20143589;MFCD27964776;AKOS028110874;EN300-1660911;Z1862027236

Chemical Property of 6-Hydroxyhexyl acrylate

Chemical Property:

• Vapor Pressure: 0.0025mmHg at 25°C
• Refractive Index: 1.452
• Boiling Point: 255.3 °C at 760 mmHg
• PKA: 15.16±0.10(Predicted)
• Flash Point: 100.6 °C
• PSA: 46.53000
• Density: 0.994 g/cm³
• LogP: 1.26830
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 8
• Exact Mass: 172.109944368
• Heavy Atom Count: 12
• Complexity: 132

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC(=O)OCCCCCCO

Technology Process of 6-Hydroxyhexyl acrylate

There total 4 articles about 6-Hydroxyhexyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,6-hexanediol (629-11-8) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → acrylic acid 6-hydroxyhexyl ester (10095-14-4)

Guidance literature:

With 10H-phenothiazine; dioctyltin(IV) oxide; In cyclohexane; at 85 ℃; Concentration; Temperature;

Reference yield:

1,6-hexanediol (629-11-8) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → hexamethylene glycol diacrylate (13048-33-4) + acrylic acid 6-hydroxyhexyl ester (10095-14-4)

Guidance literature:

With Novozyme 435; In tert-Amyl alcohol; at 50 ℃; for 120h; Inert atmosphere; Molecular sieve; Enzymatic reaction;

DOI:10.1016/j.molcatb.2009.09.008

Reference yield:

1,6-hexanediol (629-11-8) + acrylic acid (79-10-7) → acrylic acid 6-hydroxyhexyl ester (10095-14-4)

Guidance literature:

toluene-4-sulfonic acid;

upstream raw materials:

1,6-hexanediol

acrylic acid

acrylic acid methyl ester

Downstream raw materials:

2-(Hydroxy-phenyl-methyl)-acrylic acid 6-hydroxy-hexyl ester

Refernces

• 1、 Popescu, Dragos,Hoogenboom, Richard,Keul, Helmut,Moeller, Martin. "Hydroxy functional acrylate and methacrylate monomers prepared via lipase-catalyzed transacylation reactions". experimental part. p. 80 - 89. Retrieved 2010/08/20.
• 2、 Kumakura, M.,Kojima, T.,Kaetsu, I.. "FIBROUS POLYMERIC COMPOSITES IMMOBILIZING GLUCOSE OXIDASE". . p. 65 - 72. Retrieved 2007/10/02.