N-(5-Phenyl-1,3,4-thiadiazol-2(3H)-ylidene)benzenecarboximidamide

Base Information

Chemical Name:N-(5-Phenyl-1,3,4-thiadiazol-2(3H)-ylidene)benzenecarboximidamide
CAS No.:13228-81-4
Molecular Formula:C15H12N4S
Molecular Weight:280.3476
Hs Code.:
DSSTox Substance ID:DTXSID00927602

Synonyms:DTXSID00927602;13228-81-4;N-(5-Phenyl-1,3,4-thiadiazol-2(3H)-ylidene)benzenecarboximidamide

Suppliers and Price of N-(5-Phenyl-1,3,4-thiadiazol-2(3H)-ylidene)benzenecarboximidamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N-(5-Phenyl-1,3,4-thiadiazol-2(3H)-ylidene)benzenecarboximidamide

Chemical Property:

Boiling Point:482.9°Cat760mmHg
Flash Point:245.9°C
Density:1.31g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:280.07826757
Heavy Atom Count:20
Complexity:335

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=NN=C(S2)N=C(C3=CC=CC=C3)N
Isomeric SMILES:C1=CC=C(C=C1)C2=NN=C(S2)/N=C(/C3=CC=CC=C3)\N

Technology Process of N-(5-Phenyl-1,3,4-thiadiazol-2(3H)-ylidene)benzenecarboximidamide

There total 4 articles about N-(5-Phenyl-1,3,4-thiadiazol-2(3H)-ylidene)benzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2002-03-1
2-amino-5-phenyl-1,3,4-thiadiazole

: 100-47-0
benzonitrile

: 13228-81-4
N-(5-phenyl-[1,3,4]thiadiazol-2-yl)-benzamidine

Guidance literature:: With aluminium trichloride; at 180 ℃; for 5h;

Reference yield: 71.0%

: 2002-03-1
2-amino-5-phenyl-1,3,4-thiadiazole

: 41981-24-2
methyl benzenecarbimidothioate hydroiodide

: 13228-81-4
N-(5-phenyl-1,3,4-thiadiazol-2-yl) benzamidine

Guidance literature:: In methanol; for 24h; Ambient temperature;

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 13228-81-4
N-(5-phenyl-[1,3,4]thiadiazol-2-yl)-benzamidine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄

2: AlCl₃

With aluminium trichloride; sulfuric acid;
DOI:10.1021/jo01349a014