1,6-Naphthyridin-2(1H)-one, 5,7-dichloro-1-(2,6-dichlorophenyl)-

Base Information

Chemical Name:1,6-Naphthyridin-2(1H)-one, 5,7-dichloro-1-(2,6-dichlorophenyl)-
CAS No.:872973-92-7
Molecular Formula:C14H6Cl4N2O
Molecular Weight:360.026
Hs Code.:
DSSTox Substance ID:DTXSID90467562
Nikkaji Number:J2.279.946K
Wikidata:Q82294559

Synonyms:872973-92-7;1,6-NAPHTHYRIDIN-2(1H)-ONE, 5,7-DICHLORO-1-(2,6-DICHLOROPHENYL)-;DTXSID90467562

Suppliers and Price of 1,6-Naphthyridin-2(1H)-one, 5,7-dichloro-1-(2,6-dichlorophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-Naphthyridin-2(1H)-one, 5,7-dichloro-1-(2,6-dichlorophenyl)-

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:359.920473
Heavy Atom Count:21
Complexity:437

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)N2C(=O)C=CC3=C(N=C(C=C32)Cl)Cl)Cl

Technology Process of 1,6-Naphthyridin-2(1H)-one, 5,7-dichloro-1-(2,6-dichlorophenyl)-

There total 5 articles about 1,6-Naphthyridin-2(1H)-one, 5,7-dichloro-1-(2,6-dichlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872973-88-1
1-(2,6-dichlorophenyl)-6-(4-methoxybenzyl)-1,6-naphthyridone-2,5,7-(1H,6H,8H)-trione

: 872973-92-7
5,7-dichloro-1-(2,6-dichlorophenyl)-1,6-naphthyridin-2-(1H)-one

Guidance literature:: With tetramethlyammonium chloride; trichlorophosphate; at 140 ℃; for 21h;
DOI:10.1021/jo0514927

Reference yield:

: methyl 5-[(4-methoxybenzyl)amino]-3,5-dioxopentanoate

: 872973-92-7
5,7-dichloro-1-(2,6-dichlorophenyl)-1,6-naphthyridin-2-(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid monohydrate / toluene / 20 h / 117 °C

2: t-BuOK / 1-methyl-pyrrolidin-2-one; tetrahydrofuran / 3 h / 100 °C

3: POCl₃; Me₄NCl / 21 h / 140 °C

With potassium tert-butylate; tetramethlyammonium chloride; toluene-4-sulfonic acid; trichlorophosphate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; toluene;
DOI:10.1021/jo0514927

Reference yield:

: 872973-83-6
4-[(2,6-dichlorophenyl)amino]-1-(4-methoxybenzyl)pyridine-2,6-(1H,3H)-dione

: 872973-92-7
5,7-dichloro-1-(2,6-dichlorophenyl)-1,6-naphthyridin-2-(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / 1-methyl-pyrrolidin-2-one; tetrahydrofuran / 3 h / 100 °C

2: POCl₃; Me₄NCl / 21 h / 140 °C

With potassium tert-butylate; tetramethlyammonium chloride; trichlorophosphate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;
DOI:10.1021/jo0514927