N-benzyl-N-[bis[(2-methylpropan-2-yl)oxy]phosphorylmethyl]-1-phenylmethanamine

Base Information

Chemical Name:N-benzyl-N-[bis[(2-methylpropan-2-yl)oxy]phosphorylmethyl]-1-phenylmethanamine
CAS No.:873200-44-3
Molecular Formula:C23H34NO3P
Molecular Weight:403.502
Hs Code.:
Mol file:873200-44-3.mol

Synonyms:(dibenzylamino)methylphosphonic acid di-tert-butylester;

Suppliers and Price of N-benzyl-N-[bis[(2-methylpropan-2-yl)oxy]phosphorylmethyl]-1-phenylmethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-[bis[(2-methylpropan-2-yl)oxy]phosphorylmethyl]-1-phenylmethanamine

Chemical Property:

PSA：48.58000
LogP:6.46960

Purity/Quality:

Safty Information:

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Technology Process of N-benzyl-N-[bis[(2-methylpropan-2-yl)oxy]phosphorylmethyl]-1-phenylmethanamine

There total 2 articles about N-benzyl-N-[bis[(2-methylpropan-2-yl)oxy]phosphorylmethyl]-1-phenylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.3%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 15205-62-6
tri(tert-butyl)phosphite

: 873200-44-3
(dibenzylamino)methylphosphonic acid di-tert-butylester

Guidance literature:: formaldehyd; dibenzylamine; In acetonitrile; at 80 ℃; for 1h;

tri(tert-butyl)phosphite; In acetonitrile; at 20 ℃; for 22h;

Reference yield: 62.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 15205-62-6
tri(tert-butyl)phosphite

: 103-49-1
dibenzylamine

: 873200-44-3
(dibenzylamino)methylphosphonic acid di-tert-butylester

Guidance literature:: formaldehyd; dibenzylamine; In acetonitrile; at 80 ℃; for 1h;

tri(tert-butyl)phosphite; In acetonitrile; at 20 ℃; for 22.4167h;
DOI:10.1021/ol300664d

Reference yield:

: 873200-44-3
(dibenzylamino)methylphosphonic acid di-tert-butylester

: N,N'-[[[[bis(1,1-dimethylethoxy)phosphinyl]methyl]imino]di-2,1-ethanediyl]bis[N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-L-aspartic acid] 1,1'-bis(1,1-dimethylethyl) 4,4'-bis(phenylmethyl)ester

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 760.05 Torr

2: acetonitrile; aq. phosphate buffer / 30 h / pH 8

With palladium 10% on activated carbon; hydrogen; In methanol; aq. phosphate buffer; acetonitrile;
DOI:10.1039/c5ra15071j