3'-CHLORO-2,4-DINITRODIPHENYLAMINE

Base Information

• Chemical Name: 3'-CHLORO-2,4-DINITRODIPHENYLAMINE
• CAS No.: 16220-58-9
• Molecular Formula: C12H8 Cl N3 O4
• Molecular Weight: 293.666
• Hs Code.: 2921440000
• Mol file: 16220-58-9.mol

Synonyms:Diphenylamine,3'-chloro-2,4-dinitro- (8CI); 3-Chloro-2',4'-dinitrodiphenylamine;3'-Chloro-2,4-dinitrodiphenylamine; NSC 157494

Chemical Property of 3'-CHLORO-2,4-DINITRODIPHENYLAMINE

Chemical Property:

• Vapor Pressure: 1.19E-07mmHg at 25°C
• Boiling Point: 431.5°Cat760mmHg
• Flash Point: 214.8°C
• PSA: 103.67000
• Density: 1.536g/cm³
• LogP: 5.01940

Purity/Quality:

3'-CHLORO-2,4-DINITRODIPHENYLAMINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3'-CHLORO-2,4-DINITRODIPHENYLAMINE

There total 5 articles about 3'-CHLORO-2,4-DINITRODIPHENYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-aniline (108-42-9) → 2,4-dinitro-3'-chloro diphenylamine (16220-58-9) + 3-chloroaniline hydrochloride (141-85-5)

Guidance literature:

With 1-chloro-2,4-dinitro-benzene; In 1,4-dioxane; water; at 45 ℃; for 0.5h;

Reference yield:

3-chloro-aniline (108-42-9) + 1-chloro-2,4-dinitro-benzene (97-00-7) → 2,4-dinitro-3'-chloro diphenylamine (16220-58-9) + 3-chloroaniline hydrochloride (141-85-5)

Guidance literature:

In 1,4-dioxane; water; at 45 ℃; for 0.5h; Kinetics; Thermodynamic data; Product distribution; other temperatures;

Reference yield:

meta-dinitrobenzene (99-65-0) + 3-chloro-aniline (108-42-9) → 2,4-dinitro-3'-chloro diphenylamine (16220-58-9)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 0 deg C, 2 h, 2.) DMF, 0 deg C, 2 h;

DOI:10.1002/prac.19943360618

upstream raw materials:

3-chloro-aniline

1-chloro-2,4-dinitro-benzene

meta-dinitrobenzene

2,4-Dinitrofluorobenzene