4-[(4-Bromophenyl)hydrazinylidene]naphthalen-1-one

Base Information

Chemical Name:4-[(4-Bromophenyl)hydrazinylidene]naphthalen-1-one
CAS No.:6953-40-8
Molecular Formula:C16H11BrN2O
Molecular Weight:327.1753
Hs Code.:
NSC Number:71259
DSSTox Substance ID:DTXSID401258963
Nikkaji Number:J2.263.670G

Synonyms:6953-40-8;4-[(4-bromophenyl)hydrazinylidene]naphthalen-1-one;4-(4-Bromophenylazo)-1-naphthol;NSC71259;NCIOpen2_008526;DTXSID401258963;NSC-71259;AKOS003416719;AKOS003612866;4-[2-(4-Bromophenyl)diazenyl]-1-naphthalenol

Suppliers and Price of 4-[(4-Bromophenyl)hydrazinylidene]naphthalen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-[(4-Bromophenyl)hydrazinylidene]naphthalen-1-one

Chemical Property:

Vapor Pressure:3.83E-08mmHg at 25°C
Boiling Point:445.8°Cat760mmHg
Flash Point:223.4°C
Density:1.46g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:326.00548
Heavy Atom Count:20
Complexity:341

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=CC=C2O)N=NC3=CC=C(C=C3)Br

Technology Process of 4-[(4-Bromophenyl)hydrazinylidene]naphthalen-1-one

There total 5 articles about 4-[(4-Bromophenyl)hydrazinylidene]naphthalen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-15-3
α-naphthol

: C₆H₄BrN₂⁽¹⁺⁾*IO₄^(1-)

: 6953-40-8
4-(4-bromo-phenylazo)-[1]naphthol

: 66881-44-5
C₁₆H₁₁BrN₂O

Guidance literature:: In neat (no solvent); at 20 ℃;
DOI:10.4314/bcse.v27i3.13

Reference yield:

: 106-40-1
4-bromo-aniline

: 6953-40-8
4-(4-bromo-phenylazo)-[1]naphthol

: 66881-44-5
C₁₆H₁₁BrN₂O

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; water / neat (no solvent) / 20 °C

2: neat (no solvent) / 20 °C

With water; sodium nitrite; In neat (no solvent);
DOI:10.4314/bcse.v27i3.13

Reference yield:

: 90-15-3
α-naphthol

: 106-40-1
4-bromo-aniline

: 6953-40-8
4-(4-bromo-phenylazo)-[1]naphthol

Guidance literature:: 4-bromo-aniline; With hydrogenchloride; sodium nitrite; at 0 - 5 ℃;

α-naphthol; With sodium hydroxide;
DOI:10.1080/15421406.2019.1655985