1,3,4-Oxadiazole, 2-[4-(bromomethyl)phenyl]-5-(4-ethoxyphenyl)-

Base Information

Chemical Name:1,3,4-Oxadiazole, 2-[4-(bromomethyl)phenyl]-5-(4-ethoxyphenyl)-
CAS No.:873691-38-4
Molecular Formula:C17H15BrN2O2
Molecular Weight:359.21700
Hs Code.:

Synonyms:2-[(4-bromomethyl)phenyl]-5-(4-ethoxyphenyl)-1,3,4-oxadiazole;1,3,4-Oxadiazole,2-[4-(bromomethyl)phenyl]-5-(4-ethoxyphenyl);

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,4-Oxadiazole, 2-[4-(bromomethyl)phenyl]-5-(4-ethoxyphenyl)-

Chemical Property:

Melting Point:104-108 °C
Boiling Point:482.9±55.0 °C(Predicted)
PSA：48.15000
Density:1.385±0.06 g/cm3(Predicted)
LogP:4.69720

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3,4-Oxadiazole, 2-[4-(bromomethyl)phenyl]-5-(4-ethoxyphenyl)-

There total 4 articles about 1,3,4-Oxadiazole, 2-[4-(bromomethyl)phenyl]-5-(4-ethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 338426-44-1
2-(4-ethoxyphenyl)-5-(4-methyl phenyl)-1,3,4-oxadiazole

: 873691-38-4
2-[(4-bromomethyl)phenyl]-5-(4-ethoxyphenyl)-1,3,4-oxadiazole

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In benzene; for 5h; Reflux;
DOI:10.1039/c2ob26888d

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 873691-38-4
2-[(4-bromomethyl)phenyl]-5-(4-ethoxyphenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / chloroform / 3 h / Reflux

2: trichlorophosphate / 7 h / Reflux

3: N-Bromosuccinimide; dibenzoyl peroxide / benzene / 5 h / Reflux

With pyridine; N-Bromosuccinimide; trichlorophosphate; dibenzoyl peroxide; In chloroform; benzene;
DOI:10.1039/c2ob26888d

Reference yield:

: 765287-28-3
1-(4-Methylbenzoyl)-2-(4-ethyloxybenzoyl)-hydrazine

: 873691-38-4
2-[(4-bromomethyl)phenyl]-5-(4-ethoxyphenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 7 h / Reflux

2: N-Bromosuccinimide; dibenzoyl peroxide / benzene / 5 h / Reflux

With N-Bromosuccinimide; trichlorophosphate; dibenzoyl peroxide; In benzene;
DOI:10.1039/c2ob26888d