1,6-diazabicyclo[4.4.0]decane

Base Information

• Chemical Name: 1,6-diazabicyclo[4.4.0]decane
• CAS No.: 3661-15-2
• Molecular Formula: C₈H₁₆N₂
• Molecular Weight: 140.228
• Mol file: 3661-15-2.mol

Synonyms:1,6-Diazabicyclo[4.4.0]decane;10-Azaquinolizidine; 9,10-Diazadecalin; Piperidazo[1,2-a]piperidazine

Chemical Property of 1,6-diazabicyclo[4.4.0]decane

Chemical Property:

• Vapor Pressure: 0.273mmHg at 25°C
• Boiling Point: 203.7°Cat760mmHg
• Flash Point: 71.7°C
• Density: 1.02g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-diazabicyclo[4.4.0]decane

There total 7 articles about 1,6-diazabicyclo[4.4.0]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

piperidazine (505-19-1) + 1,4-dichlorobutane (110-56-5) → octahydro-pyridazino[1,2-a]pyridazine (3661-15-2)

Guidance literature:

With sodium hydroxide;

DOI:10.1002/ardp.19592920503

Reference yield:

1,4-dibromo-butane (110-52-1) → octahydro-pyridazino[1,2-a]pyridazine (3661-15-2)

Guidance literature:

With potassium hydroxide; hydrazine hydrate;

DOI:10.1007/BF00622232

Reference yield:

2,5-diketo-1,6-diazabiciclo<4.4.0>decane (3661-10-7) → octahydro-pyridazino[1,2-a]pyridazine (3661-15-2)

Guidance literature:

With lithium aluminium tetrahydride;

upstream raw materials:

piperidazine

1-methyl-4-nitrosobenzene

1,3-dibromo-propane

1,4-dichlorobutane