1-Bromo-2,5-dimethoxy-3-nitrobenzene

Base Information

Chemical Name:1-Bromo-2,5-dimethoxy-3-nitrobenzene
CAS No.:55034-12-3
Molecular Formula:C8H8 Br N O4
Molecular Weight:262.06
Hs Code.:2909309090
European Community (EC) Number:259-440-9
DSSTox Substance ID:DTXSID40203573
Nikkaji Number:J326.724E
Wikidata:Q83076971
Mol file:55034-12-3.mol

Synonyms:1-Bromo-2,5-dimethoxy-3-nitrobenzene;55034-12-3;EINECS 259-440-9;1-bromo-2,5-dimethoxy-3-nitro-benzene;SCHEMBL5038570;DTXSID40203573;QSEWGOVLIQAGQY-UHFFFAOYSA-N;1,4-Dimethoxy-2-bromo-6-nitrobenzene;CS-0254010

Suppliers and Price of 1-Bromo-2,5-dimethoxy-3-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Bromo-2,5-dimethoxy-3-nitrobenzene

Chemical Property:

Vapor Pressure:0.000112mmHg at 25°C
Melting Point:152-153 °C
Boiling Point:346.9°C at 760 mmHg
Flash Point:163.6°C
PSA：64.28000
Density:1.583g/cm³
LogP:2.89770
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:260.96367
Heavy Atom Count:14
Complexity:208

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)Br)OC)[N+](=O)[O-]

Technology Process of 1-Bromo-2,5-dimethoxy-3-nitrobenzene

There total 5 articles about 1-Bromo-2,5-dimethoxy-3-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 115929-59-4
6-bromo-4-methoxy-2-nitrophenol

: 77-78-1
dimethyl sulfate

: 55034-12-3
6-bromo-1,4-dimethoxy-2-nitrobenzene

Guidance literature:: With potassium carbonate; In acetone; for 1.5h; Heating;
DOI:10.1002/jhet.5570240629

Reference yield: 90.0%

: 115929-59-4
6-bromo-4-methoxy-2-nitrophenol

: 74-88-4
methyl iodide

: 55034-12-3
6-bromo-1,4-dimethoxy-2-nitrobenzene

Guidance literature:: With potassium hydroxide; In acetone; Reflux;
DOI:10.1021/jo302389s

Reference yield:

: 1568-70-3
4-methoxy-2-nitrophenol

: 55034-12-3
6-bromo-1,4-dimethoxy-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / AcOH; Br₂ / 1 h / Heating

2: 72 percent / K₂CO₃ / acetone / 5 h / Heating

With bromine; potassium carbonate; acetic acid; In acetone;
DOI:10.1021/ol062642i