1-Chloro-13-fluorotridecane

Base Information

• Chemical Name: 1-Chloro-13-fluorotridecane
• CAS No.: 334-75-8
• Molecular Formula: C13H26ClF
• Molecular Weight: 236.7969
• Mol file: 334-75-8.mol

Synonyms:1-Chloro-13-fluoro-tridecane;1-Chlor-13-fluor-tridecan;

Chemical Property of 1-Chloro-13-fluorotridecane

Chemical Property:

• Vapor Pressure: 0.00136mmHg at 25°C
• Boiling Point: 306.9°Cat760mmHg
• Flash Point: 146.7°C
• PSA: 0.00000
• Density: 0.91g/cm³
• LogP: 5.48580

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Chloro-13-fluorotridecane

There total 2 articles about 1-Chloro-13-fluorotridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-fluoro-decan-1-ol (334-64-5) → 1-chloro-13-fluoro-tridecane (334-75-8)

Guidance literature:

Multi-step reaction with 2 steps

1: chromium (VI)-oxide; aqueous acetic acid

2: sodium; methanol / Electrolysis_.an Platin-Elektroden

With chromium(VI) oxide; methanol; sodium; acetic acid;

DOI:10.1021/ja01591a062

Reference yield:

5-chloro-valeric acid (1119-46-6) + 10-fluorodecanoic acid (334-59-8) → 1-chloro-13-fluoro-tridecane (334-75-8)

Guidance literature:

With methanol; sodium; Electrolysis_.an Platin-Elektroden;

DOI:10.1021/ja01591a062

upstream raw materials:

5-chloro-valeric acid

10-fluorodecanoic acid

10-fluoro-decan-1-ol