1,1,12,12-Tetraphenyl-1,12-distannacyclodocosane

Base Information

Chemical Name:1,1,12,12-Tetraphenyl-1,12-distannacyclodocosane
CAS No.:87518-37-4
Molecular Formula:C₄₄H₆₀Sn₂
Molecular Weight:826.38
Hs Code.:
DSSTox Substance ID:DTXSID60531229
Wikidata:Q82402933

Synonyms:87518-37-4;1,1,12,12-Tetraphenyl-1,12-distannacyclodocosane;DTXSID60531229

Suppliers and Price of 1,1,12,12-Tetraphenyl-1,12-distannacyclodocosane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,12,12-Tetraphenyl-1,12-distannacyclodocosane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:826.27331
Heavy Atom Count:46
Complexity:624

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCCCC[Sn](CCCCCCCCCC[Sn](CCCC1)(C2=CC=CC=C2)C3=CC=CC=C3)(C4=CC=CC=C4)C5=CC=CC=C5

Technology Process of 1,1,12,12-Tetraphenyl-1,12-distannacyclodocosane

There total 1 articles about 1,1,12,12-Tetraphenyl-1,12-distannacyclodocosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 87518-49-8
1,12-dibromo-1,1,12,12-tetraphenyl-1,12-distannadodecane

: 4101-68-2
1,10-dibromodecane

: 87518-42-1
1,1,12,12,23,23,34,34-octaphenyl-1,12,23,34-tetrastannacyclotetratetracontane

: 87518-37-4
1,1,12,12-tetraphenyl-1,12-distannacyclodocosane

Guidance literature:: With iodine; magnesium; In tetrahydrofuran; (N2); to suspn. of Mg and I2 at 25°C added over 1 h soln. of Br(CH2)10Br, stirred for 4 h, sepd. from excess of Mg, diluted with THF, added over 2.5 h to Sn-compd. soln. at 0°C, allowed to warm to 25°C, stirred for 10 h; satd. aq. NH4Cl added at 0°C, aq. layer extd. (ether), combined ethereal solns. washed (satd. aq. NaCl), dried (MgSO4), filtered, concd., chromd. (MeCN/THF), recrystd. (hexane or EtOH); elem. anal.;
DOI:10.1021/om00079a003