Phosphinecarbothioamide, N,N-dimethyl-1,1-diphenyl-

Base Information

Chemical Name:Phosphinecarbothioamide, N,N-dimethyl-1,1-diphenyl-
CAS No.:87531-21-3
Molecular Formula:C15H16NPS
Molecular Weight:273.338
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphinecarbothioamide, N,N-dimethyl-1,1-diphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Phosphinecarbothioamide, N,N-dimethyl-1,1-diphenyl-

There total 2 articles about Phosphinecarbothioamide, N,N-dimethyl-1,1-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

: 65567-06-8,4541-02-0
lithium diphenylphosphide

: 87531-21-3
1-(Diphenylphosphino)-N,N-dimethylthioformamid

Guidance literature:: In tetrahydrofuran; for 14h; Ambient temperature;

Reference yield: 55.0%

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

: 829-85-6
diphenylphosphane

: 87531-21-3
1-(Diphenylphosphino)-N,N-dimethylthioformamid

Guidance literature:: With sodium; In tetrahydrofuran; at 20 ℃; for 8h;
DOI:10.1039/b007970g

Reference yield: 95.0%

: 87531-21-3
1-(Diphenylphosphino)-N,N-dimethylthioformamid

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 95797-56-1
(CO)4CrP(C₆H₅)2C(S)N(CH₃)2

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); Cr(CO)6 was irradiated in THF at 25°C under inert atmosphere, Ph2PC(S)NMe2 was added to the resulting (CO)5Cr(THF), irradiation (high pressure Hg lamp Hanau TQ 150) was continued for 8 h at -50°C; soln. was concd., layered with hexane, crystd. at -20°C; elem. anal.;
DOI:10.1016/0022-328X(84)80732-9