N-(3,5-Diacetylphenyl)acetamide

Base Information

Chemical Name:N-(3,5-Diacetylphenyl)acetamide
CAS No.:87533-50-4
Molecular Formula:C12H13NO3
Molecular Weight:219.24
Hs Code.:
DSSTox Substance ID:DTXSID20559702
Wikidata:Q82442515

Synonyms:87533-50-4;N-(3,5-DIACETYLPHENYL)ACETAMIDE;DTXSID20559702;AB06022

Suppliers and Price of N-(3,5-Diacetylphenyl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(3,5-Diacetylphenyl)acetamide

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:219.08954328
Heavy Atom Count:16
Complexity:289

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC(=CC(=C1)NC(=O)C)C(=O)C

Technology Process of N-(3,5-Diacetylphenyl)acetamide

There total 3 articles about N-(3,5-Diacetylphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 108-24-7
acetic anhydride

: 87533-49-1
3,5-diacetyl aniline

: 87533-50-4
1,3-diacetyl-5-(acetylamino)benzene

Guidance literature:: In dichloromethane; for 0.5h; Heating;
DOI:10.1021/jm00367a007

Reference yield:

: 87533-54-8
1,3-diacetyl-5-nitrobenzene

: 87533-50-4
1,3-diacetyl-5-(acetylamino)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / SnCl₂*2H₂O, conc. aq. HCl / 0.12 h / 95 °C

2: 85 percent / CH₂Cl₂ / 0.5 h / Heating

With hydrogenchloride; tin(ll) chloride; In dichloromethane;
DOI:10.1021/jm00367a007

Reference yield:

: 87555-27-9
tetraethyl 5-nitroisophthaloylbis(malonate)

: 87533-50-4
1,3-diacetyl-5-(acetylamino)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / H₂SO₄ / acetic acid; H₂O / 3.5 h / Heating

2: 89 percent / SnCl₂*2H₂O, conc. aq. HCl / 0.12 h / 95 °C

3: 85 percent / CH₂Cl₂ / 0.5 h / Heating

With hydrogenchloride; sulfuric acid; tin(ll) chloride; In dichloromethane; water; acetic acid;
DOI:10.1021/jm00367a007