1-(2-Bromoethoxy)-4-phenoxybenzene

Base Information

• Chemical Name: 1-(2-Bromoethoxy)-4-phenoxybenzene
• CAS No.: 87545-48-0
• Molecular Formula: C14H13BrO2
• Molecular Weight: 293.16
• European Community (EC) Number: 937-031-2
• DSSTox Substance ID: DTXSID80532197
• Wikidata: Q82404617

Synonyms:1-(2-bromoethoxy)-4-phenoxybenzene;87545-48-0;Benzene, 1-(2-bromoethoxy)-4-phenoxy-;SCHEMBL2291508;DTXSID80532197;DHBGFBFDCPJARX-UHFFFAOYSA-N;2-(4-phenoxyphenoxy)ethyl bromide;AKOS000199887;1-(2-Bromo-ethoxy)-4-phenoxy-benzene;CS-0263656;EN300-88665;A1-30978

Chemical Property of 1-(2-Bromoethoxy)-4-phenoxybenzene

Chemical Property:

• PSA: 18.46000
• LogP: 4.25260
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 292.00989
• Heavy Atom Count: 17
• Complexity: 196

Purity/Quality:

99% ^*data from raw suppliers

1-(2-BROMO-ETHOXY)-4-PHENOXY-BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)OC2=CC=C(C=C2)OCCBr

Technology Process of 1-(2-Bromoethoxy)-4-phenoxybenzene

There total 6 articles about 1-(2-Bromoethoxy)-4-phenoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-(4-phenoxyphenoxy)-ethanol (63066-74-0) → 1-(4-(2-bromoethoxy)phenoxy)benzene (87545-48-0)

Guidance literature:

With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 1h;

Reference yield: 80.0%

4-Phenoxyphenol (831-82-3) + ethylene dibromide (106-93-4) → 1-(4-(2-bromoethoxy)phenoxy)benzene (87545-48-0)

Guidance literature:

With potassium hydroxide; for 8h; Reflux;

DOI:10.1016/j.ejmech.2012.10.057

Reference yield:

2-(4-phenoxyphenoxy)-ethyl-tetrahydropyranyl-ether (126301-65-3) → 1-(4-(2-bromoethoxy)phenoxy)benzene (87545-48-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / methanol / 16 h / 23 °C

2: triphenylphosphine; N-Bromosuccinimide / dichloromethane / 0 °C

With N-Bromosuccinimide; pyridinium p-toluenesulfonate; triphenylphosphine; In methanol; dichloromethane;

DOI:10.1016/j.bmc.2019.02.039

upstream raw materials:

4-Phenoxyphenol

ethylene dibromide

2-(4-phenoxyphenoxy)-ethanol

2-(4-phenoxyphenoxy)-ethyl-tetrahydropyranyl-ether

Downstream raw materials:

Propan-2-one O-[2-(4-phenoxy-phenoxy)-ethyl]-oxime

C₂₀H₁₇NO₅

(S)-2-tert-Butoxycarbonylamino-3-{4-[2-(4-phenoxy-phenoxy)-ethoxy]-phenyl}-propionic acid methyl ester

3-[2-(4-Phenoxy-phenoxy)-ethoxy]-phenylamine

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