Dibenzo(b,e)(1,4)dioxin-1-carboxamide, N-(2-(dimethylamino)ethyl)-

Base Information

Chemical Name:Dibenzo(b,e)(1,4)dioxin-1-carboxamide, N-(2-(dimethylamino)ethyl)-
CAS No.:112022-10-3
Molecular Formula:C₁₇H₁₈N₂O₃
Molecular Weight:298.342
Hs Code.:
UNII:ZOY5JLU9NK
DSSTox Substance ID:DTXSID40149826
Nikkaji Number:J457.399D
Wikidata:Q27894618
ChEMBL ID:CHEMBL88776
Mol file:112022-10-3.mol

Synonyms:112022-10-3;SN-23935;Dibenzo(b,e)(1,4)dioxin-1-carboxamide, N-(2-(dimethylamino)ethyl)-;ZOY5JLU9NK;N-(2-(Dimethylamino)ethyl)dibenzo(b,e)(1,4)dioxin-1-carboxamide;CCRIS 4466;BRN 4910292;N-[2-(DIMETHYLAMINO)ETHYL]DIBENZO[B,E][1,4]DIOXIN-1-CARBOXAMIDE;UNII-ZOY5JLU9NK;N-(2-(Dimethylamino)ethyl)-dibenzo(b,e)(1,4)dioxin-1-carboxamide;CHEMBL88776;DTXSID40149826;Q27894618

Suppliers and Price of Dibenzo(b,e)(1,4)dioxin-1-carboxamide, N-(2-(dimethylamino)ethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dibenzo(b,e)(1,4)dioxin-1-carboxamide, N-(2-(dimethylamino)ethyl)-

Chemical Property:

Vapor Pressure:1.72E-07mmHg at 25°C
Boiling Point:426.8°Cat760mmHg
Flash Point:211.9°C
Density:1.216g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:298.13174244
Heavy Atom Count:22
Complexity:388

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)CCNC(=O)C1=C2C(=CC=C1)OC3=CC=CC=C3O2

Technology Process of Dibenzo(b,e)(1,4)dioxin-1-carboxamide, N-(2-(dimethylamino)ethyl)-

There total 11 articles about Dibenzo(b,e)(1,4)dioxin-1-carboxamide, N-(2-(dimethylamino)ethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 51689-37-3
methyl dibenzo<1,4>dioxin-1-carboxylate

: 108-00-9
N,N-dimethylethylenediamine

: 112022-10-3
N-<2-(dimethylamino)ethyl>dibenzo<1,4>dioxin-1-carboxamide

Guidance literature:: for 6.5h; Heating;
DOI:10.1016/0022-328X(91)86467-5

Reference yield: 11.0%

: ammonium hexafluorophosphate

: (η6-1,2-dichlorobenzene)(η5-cyclopentadienyl)iron(II) hexafluorophosphate

: 139458-18-7
2,3-dihydroxy-N-<2-(dimethylamino)ethyl>benzamide

: (η5-2,4-cyclopentadien-1-yl){5a,6,7,8,9,9a}-N-{2-(dimethylamino)ethyl}dibenzo{b,e}{1,4}dioxin-1-carboxamide}iron hexafluorophosphate

: 112022-10-3
N-<2-(dimethylamino)ethyl>dibenzo<1,4>dioxin-1-carboxamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; under N2, Fe-compd., diol and K2CO3 in DMF stirred for 6.0 h at room temp. in the dark, acidified with HCl, addn. of NH4PF6 in water, stirred; mother liquor extd. (CH2Cl2), dried (MgSO4), concd., combined with the solid, chromy. (alumina, CH2Cl2/EtOH 50:1);
DOI:10.1016/0022-328X(91)86467-5