6-Benzyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one

Base Information

Chemical Name:6-Benzyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one
CAS No.:87769-46-8
Molecular Formula:C₁₉H₁₈O₃
Molecular Weight:294.35
Hs Code.:
DSSTox Substance ID:DTXSID10523033
Wikidata:Q82388807

Synonyms:87769-46-8;6-Benzyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one;DTXSID10523033

Suppliers and Price of 6-Benzyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Benzyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:294.125594432
Heavy Atom Count:22
Complexity:438

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(OC(=C(C(=O)O1)C2=CC=CC=C2)CC3=CC=CC=C3)C

Technology Process of 6-Benzyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one

There total 2 articles about 6-Benzyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 87769-49-1
tert-butyl 3-oxo-2,4-diphenylbutanoate

: 67-64-1
acetone

: 87769-46-8
6-Benzyl-2,2-dimethyl-5-phenyl-[1,3]dioxin-4-one

Guidance literature:: With sulfuric acid; acetic anhydride; 1.) ice-cooling, 3 h, 2.) 0 deg C, 12 h;

Reference yield:

: 16537-09-0
t-butyl phenylacetate

: 87769-46-8
6-Benzyl-2,2-dimethyl-5-phenyl-[1,3]dioxin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / NaH / 2 h / 90 °C

2: 65 percent / conc. sulfuric acid, acetic anhydride / 1.) ice-cooling, 3 h, 2.) 0 deg C, 12 h

With sulfuric acid; acetic anhydride; sodium hydride;