Technology Process of Carbamic acid,
[[5-[acetyl(phenylmethyl)amino]-4-(phenylmethyl)-2-oxazolyl]methyl]-,
phenylmethyl ester
There total 6 articles about Carbamic acid,
[[5-[acetyl(phenylmethyl)amino]-4-(phenylmethyl)-2-oxazolyl]methyl]-,
phenylmethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl-ammonium chloride; sodium hydride;
1.) THF, 0 deg C, 15 min, 2.) RT, 1 h;
DOI:10.1021/ja00364a041
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 880 mg / tetrahydrofuran / 6 h / Ambient temperature
2: 69 percent / BF3*Et2O / CHCl3 / 6 h / 0 °C
3: 76 percent / 1.) NaH, Bu4NCl / 1.) THF, 0 deg C, 15 min, 2.) RT, 1 h
With
boron trifluoride diethyl etherate; tetrabutyl-ammonium chloride; sodium hydride;
In
tetrahydrofuran; chloroform;
DOI:10.1021/ja00364a041
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) NH4Cl, NH4OH, 2.) HCl gas / 1.) H2O-Et2O, RT, 2.) Et2O, 0 deg C
2: 880 mg / tetrahydrofuran / 6 h / Ambient temperature
3: 69 percent / BF3*Et2O / CHCl3 / 6 h / 0 °C
4: 76 percent / 1.) NaH, Bu4NCl / 1.) THF, 0 deg C, 15 min, 2.) RT, 1 h
With
hydrogenchloride; ammonium hydroxide; boron trifluoride diethyl etherate; tetrabutyl-ammonium chloride; sodium hydride; ammonium chloride;
In
tetrahydrofuran; chloroform;
DOI:10.1021/ja00364a041
