1-(Cyclohex-1-en-1-yl)-2,3,4-trimethoxybenzene

Base Information

• Chemical Name: 1-(Cyclohex-1-en-1-yl)-2,3,4-trimethoxybenzene
• CAS No.: 6773-00-8
• Molecular Formula: C15H20O3
• Molecular Weight: 248.322
• NSC Number: 84508
• DSSTox Substance ID: DTXSID80292663
• Wikidata: Q82031059
• Mol file: 6773-00-8.mol

Synonyms:6773-00-8;1-(cyclohex-1-en-1-yl)-2,3,4-trimethoxybenzene;NSC84508;NCIOpen2_004760;SCHEMBL557441;DTXSID80292663;NSC-84508

Chemical Property of 1-(Cyclohex-1-en-1-yl)-2,3,4-trimethoxybenzene

Chemical Property:

• Vapor Pressure: 5.76E-05mmHg at 25°C
• Boiling Point: 357°Cat760mmHg
• Flash Point: 120.4°C
• Density: 1.061g/cm³
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 248.14124450
• Heavy Atom Count: 18
• Complexity: 288

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C(=C(C=C1)C2=CCCCC2)OC)OC

Technology Process of 1-(Cyclohex-1-en-1-yl)-2,3,4-trimethoxybenzene

There total 3 articles about 1-(Cyclohex-1-en-1-yl)-2,3,4-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1-cyclohex-1-enyl-2,3,4-trimethoxy-benzene (6773-00-8)

Guidance literature:

DOI:10.1039/jr9550004435 DOI:10.1021/ja01101a025

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1-cyclohex-1-enyl-2,3,4-trimethoxy-benzene (6773-00-8)

Guidance literature:

DOI:10.1021/ja01636a013

Reference yield:

2,3,4-trimethoxybromobenzene (10385-36-1) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1-cyclohex-1-enyl-2,3,4-trimethoxy-benzene (6773-00-8)

Guidance literature:

Multistep reaction; (i) Mg, THF, (ii) /BRN= 385735/;

DOI:10.1021/jo01345a027

upstream raw materials:

2,3,4-trimethoxybromobenzene

cyclohexanone

Downstream raw materials:

1-(2',3',4'-Trimethoxyphenyl)-7-methylenebicyclo<4.1.0>heptane

trans-2-(2,3,4-Trimethoxy-phenyl)-cyclohexanol

2,3,4,6-tetrahydroxy-1,7-diphenyl-benzocyclohepten-5-one

Biphenyl-2,3,4-triol