L-Tyrosine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2-dimethylpropyl sulfate (ester)

Base Information

Chemical Name:L-Tyrosine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2-dimethylpropyl sulfate (ester)
CAS No.:878408-63-0
Molecular Formula:C₂₉H₃₁NO₈S
Molecular Weight:553.633
Hs Code.:

Synonyms:FMOC-TYR(SO2(ONEOPENTYL))-OH;L-Tyrosine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2-dimethylpropyl sulfate (ester);

Suppliers and Price of L-Tyrosine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2-dimethylpropyl sulfate (ester)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Iris Biotech GmbH
Fmoc-L-Tyr(SO3nP)-OH
5 g
$ 1215.00

Iris Biotech GmbH
Fmoc-L-Tyr(SO3nP)-OH
1 g
$ 303.75

ChemPep
Fmoc-Tyr(SO3nP)-OH
5g
$ 1500.00

Total 19 raw suppliers

Chemical Property of L-Tyrosine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2-dimethylpropyl sulfate (ester)

Chemical Property:

Boiling Point:741.0±60.0 °C(Predicted)
PSA：136.61000
Density:1.315±0.06 g/cm3(Predicted)
LogP:6.37900

Purity/Quality:

>98% ^*data from raw suppliers

Fmoc-L-Tyr(SO3nP)-OH ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of L-Tyrosine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2-dimethylpropyl sulfate (ester)

There total 4 articles about L-Tyrosine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, 2,2-dimethylpropyl sulfate (ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: Tyr(OSO₃nP)-OH

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 878408-63-0
N-(9-fluorenylmethoxycarbonyl) L-tyrosine neopentyl sulfate

Guidance literature:: With sodium carbonate; In 1,4-dioxane;
DOI:10.1039/d0ob01526a

Reference yield:

: Tyr(OSO₃nP)-OH

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 878408-63-0
N-(9-fluorenylmethoxycarbonyl) L-tyrosine neopentyl sulfate

Guidance literature:: With sodium carbonate; In 1,4-dioxane;
DOI:10.1021/ja056086j

Reference yield:

: 3978-80-1
Boc-Tyr-OH

: 878408-63-0
N-(9-fluorenylmethoxycarbonyl) L-tyrosine neopentyl sulfate

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethylformamide dineopentyl acetal / toluene

2: sodium hexamethyldisilazane

3: trifluoroacetic acid / 1 h / 20 °C

4: sodium carbonate / 1,4-dioxane

With sodium hexamethyldisilazane; sodium carbonate; N,N-dimethylformamide dineopentyl acetal; trifluoroacetic acid; In 1,4-dioxane; toluene;
DOI:10.1039/d0ob01526a