Technology Process of Benzeneethanamine, a-butyl-, (S)-
There total 7 articles about Benzeneethanamine, a-butyl-, (S)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2 / Pd/C / ethanol / 20 °C
2: HCl / diethyl ether
With
hydrogenchloride; hydrogen;
palladium on activated charcoal;
In
diethyl ether; ethanol;
DOI:10.1021/jm0613673
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aq. NaBr; NaOCl; NaHCO3 / 2,2,6,6-tetramethylpiperidine-1-yloxy free radical / toluene; ethyl acetate / -5 - 0 °C
2.1: potassium bis(trimethylsilyl)amide / toluene / 0.08 h / 0 °C
2.2: 75 percent / toluene / -78 - 20 °C
3.1: H2 / Pd/C / ethanol / 20 °C
4.1: HCl / diethyl ether
With
hydrogenchloride; sodium hypochlorite; hydrogen; potassium hexamethylsilazane; sodium hydrogencarbonate; sodium bromide;
palladium on activated charcoal;
In
diethyl ether; ethanol; ethyl acetate; toluene;
2.2: Wittig reaction;
DOI:10.1021/jm0613673
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium bis(trimethylsilyl)amide / toluene / 0.08 h / 0 °C
1.2: 75 percent / toluene / -78 - 20 °C
2.1: H2 / Pd/C / ethanol / 20 °C
3.1: HCl / diethyl ether
With
hydrogenchloride; hydrogen; potassium hexamethylsilazane;
palladium on activated charcoal;
In
diethyl ether; ethanol; toluene;
1.2: Wittig reaction;
DOI:10.1021/jm0613673