6-Bromo-3-methoxy-2-methylphenol

Base Information

Chemical Name:6-Bromo-3-methoxy-2-methylphenol
CAS No.:88010-46-2
Molecular Formula:C8H9BrO2
Molecular Weight:217.062
Hs Code.:
DSSTox Substance ID:DTXSID30547039
Wikidata:Q82425040

Synonyms:6-bromo-3-methoxy-2-methylphenol;88010-46-2;SCHEMBL2048539;DTXSID30547039

Suppliers and Price of 6-Bromo-3-methoxy-2-methylphenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 6-Bromo-3-methoxy-2-methylphenol

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:215.97859
Heavy Atom Count:11
Complexity:129

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1O)Br)OC

Technology Process of 6-Bromo-3-methoxy-2-methylphenol

There total 1 articles about 6-Bromo-3-methoxy-2-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 6971-52-4
3-methoxy-2-methylphenol

: 88010-47-3
4,6-Dibromo-3-methoxy-2-methylphenol

: 88010-46-2
6-Bromo-3-methoxy-2-methyl-phenol

Guidance literature:: With bromine; tert-butylamine; at -78 ℃;
DOI:10.1039/c39830000817

Reference yield: 75.0%

: 4885-02-3
Dichloromethyl methyl ether

: 88010-46-2
6-Bromo-3-methoxy-2-methyl-phenol

: 105104-03-8
5-Bromo-4-hydroxy-2-methoxy-3-methyl-benzaldehyde

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo00376a007

Reference yield:

: 88010-46-2
6-Bromo-3-methoxy-2-methyl-phenol

: 105104-06-1
6-bromo-3-methoxy-2-methyl-4-<(2,4-pentadienyl)oxy>phenyl

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / TiCl₄ / CH₂Cl₂ / 1 h / 0 °C

2: 74 percent / pyridine / 22 h / Ambient temperature

3: 1.) m-CPBA, 2.) KOH / 1.) CH₂Cl₂, 3 h, RT, 2.) MeOH, 1 h, 0 deg C

4: 56 percent / K₂CO₃ / acetone / 16 h / Heating

5: KOH / methanol / 3 h / 0 °C

With potassium hydroxide; titanium tetrachloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In pyridine; methanol; dichloromethane; acetone;
DOI:10.1021/jo00376a007