Technology Process of Benzeneacetaldehyde, a-(dicyclohexylhydrazono)-
There total 4 articles about Benzeneacetaldehyde, a-(dicyclohexylhydrazono)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: zinc dust, glacial acetic acid / 0.67 h / Heating
2: potassium hydroxide / ethanol / 1 h / 40 - 50 °C / pH 10
3: dimethylformamide / 12 h / Ambient temperature
4: aq. NaHCO3 / 12 h / pH 8; other 1,1-dimethyl-5,5-dialkyl-3-aryl-1,4,5-triaza-1,3-pentadienium salts, other pH, other times
With
potassium hydroxide; sodium hydrogencarbonate; acetic acid; zinc;
In
ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / ethanol / 1 h / 40 - 50 °C / pH 10
2: dimethylformamide / 12 h / Ambient temperature
3: aq. NaHCO3 / 12 h / pH 8; other 1,1-dimethyl-5,5-dialkyl-3-aryl-1,4,5-triaza-1,3-pentadienium salts, other pH, other times
With
potassium hydroxide; sodium hydrogencarbonate;
In
ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dimethylformamide / 12 h / Ambient temperature
2: aq. NaHCO3 / 12 h / pH 8; other 1,1-dimethyl-5,5-dialkyl-3-aryl-1,4,5-triaza-1,3-pentadienium salts, other pH, other times
With
sodium hydrogencarbonate;
In
N,N-dimethyl-formamide;