1-Phenylglyoxal-2-dicyclohexylhydrazon

Base Information

Chemical Name:1-Phenylglyoxal-2-dicyclohexylhydrazon
CAS No.:88026-84-0
Molecular Formula:C₂₀H₂₈N₂O
Molecular Weight:312.455
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenylglyoxal-2-dicyclohexylhydrazon

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Technology Process of 1-Phenylglyoxal-2-dicyclohexylhydrazon

There total 5 articles about 1-Phenylglyoxal-2-dicyclohexylhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 88026-83-9
1-Phenylglyoxal-1-dicyclohexylhydrazon

: 88026-84-0
1-Phenylglyoxal-2-dicyclohexylhydrazon

Guidance literature:: With sulfuric acid; In ethanol; for 3h; Heating;

Reference yield:

: 947-92-2
N-nitrosodicyclohexylamine

: 88026-84-0
1-Phenylglyoxal-2-dicyclohexylhydrazon

Guidance literature:: Multi-step reaction with 5 steps

1: zinc dust, glacial acetic acid / 0.67 h / Heating

2: potassium hydroxide / ethanol / 1 h / 40 - 50 °C / pH 10

3: dimethylformamide / 12 h / Ambient temperature

4: aq. NaHCO₃ / 12 h / pH 8; other 1,1-dimethyl-5,5-dialkyl-3-aryl-1,4,5-triaza-1,3-pentadienium salts, other pH, other times

5: 50 percent / 20 percent H₂SO₄ / ethanol / 3 h / Heating

With potassium hydroxide; sulfuric acid; sodium hydrogencarbonate; acetic acid; zinc; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 82259-52-7
1,1-dicyclohexylhydrazine

: 88026-84-0
1-Phenylglyoxal-2-dicyclohexylhydrazon

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / ethanol / 1 h / 40 - 50 °C / pH 10

2: dimethylformamide / 12 h / Ambient temperature

3: aq. NaHCO₃ / 12 h / pH 8; other 1,1-dimethyl-5,5-dialkyl-3-aryl-1,4,5-triaza-1,3-pentadienium salts, other pH, other times

4: 50 percent / 20 percent H₂SO₄ / ethanol / 3 h / Heating

With potassium hydroxide; sulfuric acid; sodium hydrogencarbonate; In ethanol; N,N-dimethyl-formamide;