2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]-3-methylbutan-1-ol

Base Information

Chemical Name:2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]-3-methylbutan-1-ol
CAS No.:88062-51-5
Molecular Formula:C12H16Cl2O2S
Molecular Weight:295.23
Hs Code.:
DSSTox Substance ID:DTXSID30579350

Synonyms:88062-51-5;DTXSID30579350;2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]-3-methylbutan-1-ol

Suppliers and Price of 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]-3-methylbutan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]-3-methylbutan-1-ol

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:294.0248063
Heavy Atom Count:17
Complexity:229

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)C(CO)SC1=C(C(=C(C=C1)OC)Cl)Cl

Technology Process of 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]-3-methylbutan-1-ol

There total 5 articles about 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]-3-methylbutan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 83119-44-2
α-(2,3-dichloro-4-methoxyphenylthio)isovaleric acid

: 88062-51-5
2-<(2,3-dichloro-4-methoxy)phenylthio>-3-methylbutanol

Guidance literature:: With borane; In tetrahydrofuran; for 1h; Heating;
DOI:10.1002/jhet.5570200406

Reference yield:

: 10323-40-7,565-74-2
2-bromoisovaleric acid

: 88062-51-5
2-<(2,3-dichloro-4-methoxy)phenylthio>-3-methylbutanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) sodium hydride; 2) 3N HCl / 1) DMF, 10 min; 2) room temp., 3 h

2: 97 percent / 0.94 N borane / tetrahydrofuran / 1 h / Heating

With hydrogenchloride; borane; sodium hydride; In tetrahydrofuran;
DOI:10.1002/jhet.5570200406

Reference yield:

: 1984-59-4
2,3-dichloroanisole

: 88062-51-5
2-<(2,3-dichloro-4-methoxy)phenylthio>-3-methylbutanol

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / chlorosulfonic acid / 1 h / Ambient temperature

2: 88 percent / conc. sulfuric acid, zinc dust / H₂O / 16 h / Heating

3: 1) sodium hydride; 2) 3N HCl / 1) DMF, 10 min; 2) room temp., 3 h

4: 97 percent / 0.94 N borane / tetrahydrofuran / 1 h / Heating

With hydrogenchloride; chlorosulfonic acid; sulfuric acid; borane; sodium hydride; zinc; In tetrahydrofuran; water;
DOI:10.1002/jhet.5570200406