Benzamide, 2-(dimethylamino)-N,N-diethyl-

Base Information

Chemical Name:Benzamide, 2-(dimethylamino)-N,N-diethyl-
CAS No.:88132-08-5
Molecular Formula:C13H20N2O
Molecular Weight:220.315
Hs Code.:
DSSTox Substance ID:DTXSID50446858
Nikkaji Number:J2.321.863A

Synonyms:N,N-diethyl-2-(dimethylamino)benzamide;Benzamide, 2-(dimethylamino)-N,N-diethyl-;88132-08-5;SCHEMBL7281533;DTXSID50446858;UZUPYNAQIMGZMO-UHFFFAOYSA-N

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzamide, 2-(dimethylamino)-N,N-diethyl-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:220.157563266
Heavy Atom Count:16
Complexity:224

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=CC=CC=C1N(C)C

Technology Process of Benzamide, 2-(dimethylamino)-N,N-diethyl-

There total 4 articles about Benzamide, 2-(dimethylamino)-N,N-diethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76854-95-0
2-amino-N,N-diethylbenzamide

: 74-88-4
methyl iodide

: 88132-08-5
2-(N',N'-dimethylamino)-N,N-diethylbenzamide

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 17h; Heating;
DOI:10.1021/jo0106748

Reference yield: 20.0%

: 14216-18-3
N,N-Diethyl-N',N'-dimethylharnstoff

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 88132-08-5
2-(N',N'-dimethylamino)-N,N-diethylbenzamide

: 2-(dimethylcarbamoyl)phenyl triflate

Guidance literature:: With cesium fluoride; at 50 ℃; for 10h;
DOI:10.1002/1521-3773(20020902)41:17<3247::AID-ANIE3247>3.0.CO;2-P

Reference yield:

: 610-16-2
N,N-dimethylanthranilic acid

: 88132-08-5
2-(N',N'-dimethylamino)-N,N-diethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 0.5 h

2: 3.33 g / CH₂Cl₂ / 3 h / 0 °C

With thionyl chloride; In dichloromethane;
DOI:10.1039/b600181e