Butanoic acid, 2-(phenylmethylene)-, (Z)-

Base Information

Chemical Name:Butanoic acid, 2-(phenylmethylene)-, (Z)-
CAS No.:88153-39-3
Molecular Formula:C11H12O2
Molecular Weight:176.215
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Butanoic acid, 2-(phenylmethylene)-, (Z)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanoic acid, 2-(phenylmethylene)-, (Z)-

There total 4 articles about Butanoic acid, 2-(phenylmethylene)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 100-52-7
benzaldehyde

: 107-92-6
butyric acid

: 88153-39-3
(Z)-2-benzylidenebutanoic acid

Guidance literature:: benzaldehyde; butyric acid; With titanium tetrachloride; In tetrahydrofuran; for 0.5h; Cooling;

With triethylamine; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1039/d0ob02417a

Reference yield:

: 97-94-9
triethyl borane

: 124-38-9,18923-20-1
carbon dioxide

: 536-74-3
phenylacetylene

: 26197-64-8
(E)-2-benzylidenebutanoic acid

: 88153-39-3
(Z)-2-benzylidenebutanoic acid

Guidance literature:: With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium ethoxide; In tetrahydrofuran; 1,4-dioxane; at 20 ℃; for 24h; under 760.051 Torr; Overall yield = 50 %; stereoselective reaction;
DOI:10.1021/acs.orglett.6b03860

Reference yield:

: 88153-39-3
(Z)-2-benzylidenebutanoic acid

Guidance literature:: With diethyl ether; lithium; at -20 ℃; Eintragen des Reaktionsgemisches in ein Gemisch von festem Kohlendioxid und Aether; Reinigung ueber das Anilin-Salz;