2H-Benzimidazol-2-one, 1,3-dihydro-3-(4-aminophenyl)-5-chloro-1-methyl-

Base Information

Chemical Name:2H-Benzimidazol-2-one, 1,3-dihydro-3-(4-aminophenyl)-5-chloro-1-methyl-
CAS No.:79759-75-4
Molecular Formula:C14H12ClN3O
Molecular Weight:273.7176
Hs Code.:
DSSTox Substance ID:DTXSID00229895
Wikidata:Q83110267

Synonyms:BRN 5575529;2H-Benzimidazol-2-one, 1,3-dihydro-3-(4-aminophenyl)-5-chloro-1-methyl-;79759-75-4;1,3-Dihydro-3-(4-aminophenyl)-5-chloro-1-methyl-2H-benzimidazol-2-one;DTXSID00229895;LS-33280

Suppliers and Price of 2H-Benzimidazol-2-one, 1,3-dihydro-3-(4-aminophenyl)-5-chloro-1-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2H-Benzimidazol-2-one, 1,3-dihydro-3-(4-aminophenyl)-5-chloro-1-methyl-

Chemical Property:

Vapor Pressure:1.32E-09mmHg at 25°C
Boiling Point:486.2°Cat760mmHg
Flash Point:247.8°C
Density:1.399g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:273.0668897
Heavy Atom Count:19
Complexity:357

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)Cl)N(C1=O)C3=CC=C(C=C3)N

Technology Process of 2H-Benzimidazol-2-one, 1,3-dihydro-3-(4-aminophenyl)-5-chloro-1-methyl-

There total 3 articles about 2H-Benzimidazol-2-one, 1,3-dihydro-3-(4-aminophenyl)-5-chloro-1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 79759-73-2
5-Chloro-1-methyl-3-(4-nitro-phenyl)-1,3-dihydro-benzoimidazol-2-one

: 79759-75-4
3-(4-Amino-phenyl)-5-chloro-1-methyl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: With hydrogenchloride; zinc; In ethanol; for 1h;

Reference yield:

: 586-78-7
para-nitrophenyl bromide

: 79759-75-4
3-(4-Amino-phenyl)-5-chloro-1-methyl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / AcOK, Cu, CuCl / bis-(2-methoxy-ethyl) ether / 10 h / Heating

2: 85 percent / 37 percent aq. HCl, zinc / ethanol / 1 h

With hydrogenchloride; potassium acetate; copper; copper(l) chloride; zinc; In ethanol; diethylene glycol dimethyl ether;

Reference yield:

: 15965-71-6
5-chloro-1,3-dihydro-1-methyl-2H-benzimidazol-2-one

: 79759-75-4
3-(4-Amino-phenyl)-5-chloro-1-methyl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / AcOK, Cu, CuCl / bis-(2-methoxy-ethyl) ether / 10 h / Heating

2: 85 percent / 37 percent aq. HCl, zinc / ethanol / 1 h

With hydrogenchloride; potassium acetate; copper; copper(l) chloride; zinc; In ethanol; diethylene glycol dimethyl ether;