3-Methyl-9-(pentachlorophenyl)-9H-fluoren-9-ol

Base Information

Chemical Name:3-Methyl-9-(pentachlorophenyl)-9H-fluoren-9-ol
CAS No.:88180-15-8
Molecular Formula:C20H11Cl5O
Molecular Weight:444.572
Hs Code.:
DSSTox Substance ID:DTXSID30531079

Synonyms:88180-15-8;3-Methyl-9-(pentachlorophenyl)-9H-fluoren-9-ol;DTXSID30531079

Suppliers and Price of 3-Methyl-9-(pentachlorophenyl)-9H-fluoren-9-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Methyl-9-(pentachlorophenyl)-9H-fluoren-9-ol

Chemical Property:

XLogP3:7.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:443.922303
Heavy Atom Count:26
Complexity:516

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)C(C3=CC=CC=C32)(C4=C(C(=C(C(=C4Cl)Cl)Cl)Cl)Cl)O

Technology Process of 3-Methyl-9-(pentachlorophenyl)-9H-fluoren-9-ol

There total 1 articles about 3-Methyl-9-(pentachlorophenyl)-9H-fluoren-9-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118-74-1,67471-27-6
hexachlorobenzene

: 1705-89-1
3-methyl-9H-fluoren-9-one

: 88180-15-8
3-Methyl-9-(pentachlorophenyl)-9-fluorenol

Guidance literature:: With magnesium; Yield given. Multistep reaction; 1.) THF, 2.) 24 h;
DOI:10.1021/jo00179a007

Reference yield: 94.5%

: 88180-15-8
3-Methyl-9-(pentachlorophenyl)-9-fluorenol

: 88180-16-9
3-Methyl-9-(pentachlorophenyl)fluorene

Guidance literature:: With hydrogen iodide; In acetic acid; for 17h; Heating;
DOI:10.1021/jo00179a007

Reference yield:

: 88180-15-8
3-Methyl-9-(pentachlorophenyl)-9-fluorenol

: 88180-17-0
9H-3-Methyldodecachloro-9-phenylfluorene

Guidance literature:: Multi-step reaction with 2 steps

1: 94.5 percent / 57percent aq. HI / acetic acid / 17 h / Heating

2: 64 percent / S₂Cl₂, AlCl₃ / SO₂Cl₂ / 0.08 h / Heating

With disulfur dichloride; aluminium trichloride; hydrogen iodide; In sulfuryl dichloride; acetic acid;
DOI:10.1021/jo00179a007