4-(3-Methoxy-2-methylphenoxy)-3-nitropyridine

Base Information

Chemical Name:4-(3-Methoxy-2-methylphenoxy)-3-nitropyridine
CAS No.:88220-09-1
Molecular Formula:C13H12N2O4
Molecular Weight:260.249
Hs Code.:
DSSTox Substance ID:DTXSID80530895
Wikidata:Q82402328

Synonyms:4-(3-Methoxy-2-methylphenoxy)-3-nitropyridine;88220-09-1;DTXSID80530895

Suppliers and Price of 4-(3-Methoxy-2-methylphenoxy)-3-nitropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-(3-Methoxy-2-methylphenoxy)-3-nitropyridine

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:260.07970687
Heavy Atom Count:19
Complexity:308

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC=C1OC2=C(C=NC=C2)[N+](=O)[O-])OC

Technology Process of 4-(3-Methoxy-2-methylphenoxy)-3-nitropyridine

There total 1 articles about 4-(3-Methoxy-2-methylphenoxy)-3-nitropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6971-52-4
3-methoxy-2-methylphenol

: 13091-23-1
4-chloro-3-nitropyridine

: 88220-09-1
4-(3-methoxy-2-methylphenoxy)-3-nitropyridine

Guidance literature:: With potassium hydroxide; Yield given. Multistep reaction; 1.) alcohol, 2.) DMF, room temperature, 1 h, 60 deg C, 1 h;
DOI:10.1039/P19830000225

Reference yield: 70.0%

: 88220-09-1
4-(3-methoxy-2-methylphenoxy)-3-nitropyridine

: 88220-10-4
3-amino-4-(3-methoxy-2-methylphenoxy)pyridine

Guidance literature:: With hydrogen; nickel; In ethanol; Ambient temperature;
DOI:10.1039/P19830000225

Reference yield:

: 88220-09-1
4-(3-methoxy-2-methylphenoxy)-3-nitropyridine

: 3-chloro-4-(3-methoxy-2-methylphenoxy)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / hydrogen / Raney nickel / ethanol / Ambient temperature

2: 1.) sodium nitrite, hydrochloric acid, 2.) cupric chloride / 1.) water, 0 deg C, 15 min, 2.) water, acetone, 35-40 deg C, 15 min, reflux, 5 min

With hydrogenchloride; hydrogen; copper dichloride; sodium nitrite; nickel; In ethanol;
DOI:10.1039/P19830000225