2-Butenoic acid, 3-phenyl-4-(phenylthio)-, methyl ester

Base Information

Chemical Name:2-Butenoic acid, 3-phenyl-4-(phenylthio)-, methyl ester
CAS No.:88328-80-7
Molecular Formula:C17H16O2S
Molecular Weight:284.379
Hs Code.:

Synonyms:

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Chemical Property of 2-Butenoic acid, 3-phenyl-4-(phenylthio)-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2-Butenoic acid, 3-phenyl-4-(phenylthio)-, methyl ester

There total 4 articles about 2-Butenoic acid, 3-phenyl-4-(phenylthio)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 67-56-1
methanol

: 108378-56-9
4-phenyl-4-phenylthio-4,5-dihydrofuran-2(3H)-one

: 88328-80-7
methyl 3-phenyl-4-phenylthiobut-2-enoate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 144h; Heating;

Reference yield:

: 51256-38-3
methyl α-phenyl-α-(phenylthio)acetate

: 88328-80-7
methyl 3-phenyl-4-phenylthiobut-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium di-isopropylamide / 1.) hexane/THF, 0 deg C, 2.) THF, 0 deg C, 30 min; room temperature, 48 h

2: 1.) 50 percent sodium hyride, 2.) lithium aluminium hydride / 1.) THF/oil, 0.5 h, 2.) 3 h

3: 87 percent / toluene-p-sulphonic acid monohydrate / benzene / 144 h / Heating

With lithium aluminium tetrahydride; sodium hydride; toluene-4-sulfonic acid; lithium diisopropyl amide; In benzene;

Reference yield:

: 2-bromo-2-phenylthioacetic acid

: 88328-80-7
methyl 3-phenyl-4-phenylthiobut-2-enoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) potassium hydroxide, 2.) conc. H₂SO₄ / 1.) ethanol, 0 deg C; 24 h, room temperature, 2.) room temperature, 3 d

2: 1.) lithium di-isopropylamide / 1.) hexane/THF, 0 deg C, 2.) THF, 0 deg C, 30 min; room temperature, 48 h

3: 1.) 50 percent sodium hyride, 2.) lithium aluminium hydride / 1.) THF/oil, 0.5 h, 2.) 3 h

4: 87 percent / toluene-p-sulphonic acid monohydrate / benzene / 144 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; sodium hydride; toluene-4-sulfonic acid; lithium diisopropyl amide; In benzene;