4-Chloro-N-(2-(furan-3-yl)-2-oxoethyl)benzamide

Base Information

Chemical Name:4-Chloro-N-(2-(furan-3-yl)-2-oxoethyl)benzamide
CAS No.:88352-91-4
Molecular Formula:C13H10ClNO3
Molecular Weight:263.68
Hs Code.:
DSSTox Substance ID:DTXSID20549007
Wikidata:Q82427870

Synonyms:88352-91-4;4-Chloro-N-(2-(furan-3-yl)-2-oxoethyl)benzamide;4-Chloro-N-[2-(furan-3-yl)-2-oxoethyl]benzamide;SCHEMBL10506893;DTXSID20549007;LEPLGTJRKGCSTN-UHFFFAOYSA-N;N-(4-chlorobenzoyl)-(3-furylcarbonyl)methylamine

Suppliers and Price of 4-Chloro-N-(2-(furan-3-yl)-2-oxoethyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Chloro-N-(2-(furan-3-yl)-2-oxoethyl)benzamide

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:263.0349209
Heavy Atom Count:18
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=O)NCC(=O)C2=COC=C2)Cl

Technology Process of 4-Chloro-N-(2-(furan-3-yl)-2-oxoethyl)benzamide

There total 1 articles about 4-Chloro-N-(2-(furan-3-yl)-2-oxoethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 122-01-0
4-chloro-benzoyl chloride

: 88352-90-3
aminomethyl 3-furyl ketone hydrochloride

: 88352-91-4
N-<(4-chlorobenzoyl)amino>methyl 3-furyl ketone

Guidance literature:: With sodium hydrogencarbonate;

Reference yield: 77.3%

: 105-36-2
ethyl bromoacetate

: 88352-91-4
N-<(4-chlorobenzoyl)amino>methyl 3-furyl ketone

: 88352-61-8
ethyl 3--4-(3-furyl)-4-oxobutyrate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; paraffin; 1.) -50 - -40 deg C, 20 min, 2.) -40 to 10 deg C, 30 min;
DOI:10.1021/jm00401a021

Reference yield:

: 88352-91-4
N-<(4-chlorobenzoyl)amino>methyl 3-furyl ketone

: 88352-75-4
2-[2-(4-chlorophenyl)-5-(furan-3-yl)-4-oxazolyl]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / NaH / paraffin; dimethylformamide / 1.) -50 - -40 deg C, 20 min, 2.) -40 to 10 deg C, 30 min

2: 86 percent / phosphoryl chloride / dimethylformamide / 8 h / Ambient temperature

3: 88 percent / KOH / methanol; H₂O / 8 h / 50 °C

With potassium hydroxide; sodium hydride; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide; paraffin;
DOI:10.1021/jm00401a021