(5E)-5-[2-(4-Bromophenyl)hydrazinylidene]-1-(2-chlorophenyl)-3-phenyl-2-sulfanylidenedihydropyrimidine-4,6(1H,5H)-dione

Base Information

Chemical Name:(5E)-5-[2-(4-Bromophenyl)hydrazinylidene]-1-(2-chlorophenyl)-3-phenyl-2-sulfanylidenedihydropyrimidine-4,6(1H,5H)-dione
CAS No.:76153-21-4
Molecular Formula:C₂₂H₁₄BrClN₄O₂S
Molecular Weight:513.802
Hs Code.:
NSC Number:161289,295736
DSSTox Substance ID:DTXSID80507668
Wikidata:Q82364030

Synonyms:76153-21-4;NSC161289;DTXSID80507668;NSC295736;NSC-161289;NSC-295736;(5E)-5-[2-(4-Bromophenyl)hydrazinylidene]-1-(2-chlorophenyl)-3-phenyl-2-sulfanylidenedihydropyrimidine-4,6(1H,5H)-dione

Suppliers and Price of (5E)-5-[2-(4-Bromophenyl)hydrazinylidene]-1-(2-chlorophenyl)-3-phenyl-2-sulfanylidenedihydropyrimidine-4,6(1H,5H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (5E)-5-[2-(4-Bromophenyl)hydrazinylidene]-1-(2-chlorophenyl)-3-phenyl-2-sulfanylidenedihydropyrimidine-4,6(1H,5H)-dione

Chemical Property:

Vapor Pressure:6.4E-14mmHg at 25°C
Boiling Point:590.5°Cat760mmHg
Flash Point:310.9°C
Density:1.56g/cm³
XLogP3:6.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:511.97094
Heavy Atom Count:31
Complexity:750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C(=O)C(=C(N(C2=S)C3=CC=CC=C3Cl)O)N=NC4=CC=C(C=C4)Br

Technology Process of (5E)-5-[2-(4-Bromophenyl)hydrazinylidene]-1-(2-chlorophenyl)-3-phenyl-2-sulfanylidenedihydropyrimidine-4,6(1H,5H)-dione

There total 2 articles about (5E)-5-[2-(4-Bromophenyl)hydrazinylidene]-1-(2-chlorophenyl)-3-phenyl-2-sulfanylidenedihydropyrimidine-4,6(1H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1932-36-1
1-(2-chloro-phenyl)-3-phenyl-thiourea

: 76153-21-4
5-(4-Bromo-phenylazo)-3-(2-chloro-phenyl)-6-hydroxy-1-phenyl-2-thioxo-2,3-dihydro-1H-pyrimidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: NaOEt / ethanol / 8 h / Heating

2: 1) NaNO₂, 3N HCl 2) NaOAc / 1) water, 0-5 deg C 2) EtOH, 2h, room temperature

With hydrogenchloride; sodium ethanolate; sodium acetate; sodium nitrite; In ethanol;

Reference yield:

: 76153-58-7
1-Phenyl-3-(o-chlorophenyl)-2-thiobarbituric acid

: 106-40-1
4-bromo-aniline

: 76153-21-4
5-(4-Bromo-phenylazo)-3-(2-chloro-phenyl)-6-hydroxy-1-phenyl-2-thioxo-2,3-dihydro-1H-pyrimidin-4-one

Guidance literature:: With hydrogenchloride; sodium acetate; sodium nitrite; Yield given. Multistep reaction; 1) water, 0-5 deg C 2) EtOH, 2h, room temperature;