2-Amino-N-(2-chloro-1-oxo-1lambda~5~-pyridin-3-yl)benzamide

Base Information

Chemical Name:2-Amino-N-(2-chloro-1-oxo-1lambda~5~-pyridin-3-yl)benzamide
CAS No.:88369-72-6
Molecular Formula:C12H10ClN3O2
Molecular Weight:263.683
Hs Code.:
DSSTox Substance ID:DTXSID50521573
Wikidata:Q82386120

Synonyms:88369-72-6;DTXSID50521573;2-Amino-N-(2-chloro-1-oxo-1lambda~5~-pyridin-3-yl)benzamide

Suppliers and Price of 2-Amino-N-(2-chloro-1-oxo-1lambda~5~-pyridin-3-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Amino-N-(2-chloro-1-oxo-1lambda~5~-pyridin-3-yl)benzamide

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:263.0461543
Heavy Atom Count:18
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NC2=C([N+](=CC=C2)[O-])Cl)N

Technology Process of 2-Amino-N-(2-chloro-1-oxo-1lambda~5~-pyridin-3-yl)benzamide

There total 4 articles about 2-Amino-N-(2-chloro-1-oxo-1lambda~5~-pyridin-3-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84446-16-2
3-(2'-chlorobenzoyl)amino-2-chloropyridine 1-oxide

: 88369-72-6
3-(2'-aminobenzoyl)amino-2-chloropyridine 1-oxide

Guidance literature:: With ammonium hydroxide; copper(II) sulfate; sodium chloride; at 80 ℃; for 5h;

Reference yield:

: 84446-15-1
3-(2'-bromobenzoyl)amino-2-chloropyridine 1-oxide

: 88369-72-6
3-(2'-aminobenzoyl)amino-2-chloropyridine 1-oxide

Guidance literature:: With ammonium hydroxide; copper(II) sulfate; sodium chloride; at 60 ℃; for 3h;

Reference yield:

: 84446-21-9
3-(2'-chlorobenzoyl)amino-2-chloropyridine

: 88369-72-6
3-(2'-aminobenzoyl)amino-2-chloropyridine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 40percent H₂O₂, acetic acid / 24 h / 55 - 60 °C / bath temperature

2: 8.96 g / conc. NH₄OH, CuSO₄*5H₂O, NaCl / 5 h / 80 °C

With ammonium hydroxide; dihydrogen peroxide; copper(II) sulfate; acetic acid; sodium chloride;