2-[(Z)-(3-Amino-1-hydroxypyridin-2(1H)-ylidene)amino]benzoic acid

Base Information

Chemical Name:2-[(Z)-(3-Amino-1-hydroxypyridin-2(1H)-ylidene)amino]benzoic acid
CAS No.:88369-79-3
Molecular Formula:C12H11N3O3
Molecular Weight:245.238
Hs Code.:
DSSTox Substance ID:DTXSID10521579

Synonyms:88369-79-3;DTXSID10521579;2-[(Z)-(3-Amino-1-hydroxypyridin-2(1H)-ylidene)amino]benzoic acid

Suppliers and Price of 2-[(Z)-(3-Amino-1-hydroxypyridin-2(1H)-ylidene)amino]benzoic acid

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Chemical Property of 2-[(Z)-(3-Amino-1-hydroxypyridin-2(1H)-ylidene)amino]benzoic acid

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:245.08004122
Heavy Atom Count:18
Complexity:428

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)O)N=C2C(=CC=CN2O)N

Technology Process of 2-[(Z)-(3-Amino-1-hydroxypyridin-2(1H)-ylidene)amino]benzoic acid

There total 8 articles about 2-[(Z)-(3-Amino-1-hydroxypyridin-2(1H)-ylidene)amino]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 84446-18-4
1-oxo-5,11-dihydro-6H-pyrido<2,3-b><1,4>benzodiazepin-6-one

: 88369-79-3
3-amino-2-(2'-carboxyphenyl)aminopyridine N-oxide

Guidance literature:: With potassium hydroxide; tetrabutyl-ammonium chloride; In toluene; for 4h; Heating;

Reference yield:

: 84446-21-9
3-(2'-chlorobenzoyl)amino-2-chloropyridine

: 88369-79-3
3-amino-2-(2'-carboxyphenyl)aminopyridine N-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 40percent H₂O₂, acetic acid / 24 h / 55 - 60 °C / bath temperature

2: 8.96 g / conc. NH₄OH, CuSO₄*5H₂O, NaCl / 5 h / 80 °C

3: 96 percent / 5percent aq. HCl / various solvent(s) / 1.5 h / 110 °C / bath temperature

4: 65 percent / 50percent aq. KOH / tetrabutylammonium chloride / toluene / 4 h / Heating

With hydrogenchloride; potassium hydroxide; ammonium hydroxide; dihydrogen peroxide; copper(II) sulfate; acetic acid; sodium chloride; tetrabutyl-ammonium chloride; In toluene;

Reference yield:

: 84446-17-3
3-(2'-bromobenzoyl)amino-2-chloropyridine

: 88369-79-3
3-amino-2-(2'-carboxyphenyl)aminopyridine N-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 40percent H₂O₂, acetic acid / 24 h / 55 - 60 °C / bath temperature

2: conc. NH₄OH, CuSO₄*5H₂O, NaCl / 3 h / 60 °C

3: 96 percent / 5percent aq. HCl / various solvent(s) / 1.5 h / 110 °C / bath temperature

4: 65 percent / 50percent aq. KOH / tetrabutylammonium chloride / toluene / 4 h / Heating

With hydrogenchloride; potassium hydroxide; ammonium hydroxide; dihydrogen peroxide; copper(II) sulfate; acetic acid; sodium chloride; tetrabutyl-ammonium chloride; In toluene;